Nondestructive Methodology for Identification of Local Discontinuities in Aluminide Layer-Coated MAR 247 during Its Fatigue Performance

• Main Authors: Dominik Kukla, Mateusz Kopec, Kehuan Wang, Cezary Senderowski, Zbigniew L. Kowalewski
• Format: Article
• Language: English
• Published: MDPI AG 2021-07-01
• Series: Materials
• Subjects: chemical vapor deposition; nickel alloys; aluminide coatings; fatigue; eddy current
• Online Access: https://www.mdpi.com/1996-1944/14/14/3824

In this paper, the fatigue performance of the aluminide layer-coated and as-received MAR 247 nickel superalloy with three different initial microstructures (fine grain, coarse grain and column-structured grain) was monitored using nondestructive, eddy current methods. The aluminide layers of 20 and 40 µm were obtained through the chemical vapor deposition (CVD) process in the hydrogen protective atmosphere for 8 and 12 h at the temperature of 1040 °C and internal pressure of 150 mbar. A microstructure of MAR 247 nickel superalloy and the coating were characterized using light optical microscopy (LOM), scanning electron microscopy (SEM) and X-ray energy dispersive spectroscopy (EDS). It was found that fatigue performance was mainly driven by the initial microstructure of MAR 247 nickel superalloy and the thickness of the aluminide layer. Furthermore, the elaborated methodology allowed in situ eddy current measurements that enabled us to localize the area with potential crack initiation and its propagation during 60,000 loading cycles.