A surprising new route to 4-nitro-3-phenylisoxazole

A one-pot synthesis of 4-nitro-3-phenylisoxazole has been carried out by treatment of cinnamyl alcohol dissolved in acetic acid with sodium nitrite; in addition, 4-phenyl-3-furoxanmethanol was obtained in 40% yield.

Bibliographic Details
Main Authors:	Henning Hopf, Aboul-fetouh E. Mourad, Peter G. Jones
Format:	Article
Language:	English
Published:	Beilstein-Institut 2010-06-01
Series:	Beilstein Journal of Organic Chemistry
Subjects:	cinnamyl alcohol furoxan derivatives isoxazole derivatives X-ray diffraction
Online Access:	https://doi.org/10.3762/bjoc.6.68

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spelling	doaj-be82cea3cb5a45e9a2ec512c199b9e732021-02-02T08:00:15ZengBeilstein-InstitutBeilstein Journal of Organic Chemistry1860-53972010-06-01616810.3762/bjoc.6.681860-5397-6-68A surprising new route to 4-nitro-3-phenylisoxazoleHenning Hopf0Aboul-fetouh E. Mourad1Peter G. Jones2Institut für Organische Chemie, Technische Universität Braunschweig, Postfach 3329, D-38023 Braunschweig, GermanyChemistry Department, Faculty of Science, Minia University, 61519 El-Minia, EgyptInstitut für Anorganische und Analytische Chemie, Technische Universität Braunschweig, Postfach 3329, D-38023 Braunschweig, GermanyA one-pot synthesis of 4-nitro-3-phenylisoxazole has been carried out by treatment of cinnamyl alcohol dissolved in acetic acid with sodium nitrite; in addition, 4-phenyl-3-furoxanmethanol was obtained in 40% yield.https://doi.org/10.3762/bjoc.6.68cinnamyl alcoholfuroxan derivativesisoxazole derivativesX-ray diffraction
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Henning Hopf Aboul-fetouh E. Mourad Peter G. Jones
spellingShingle	Henning Hopf Aboul-fetouh E. Mourad Peter G. Jones A surprising new route to 4-nitro-3-phenylisoxazole Beilstein Journal of Organic Chemistry cinnamyl alcohol furoxan derivatives isoxazole derivatives X-ray diffraction
author_facet	Henning Hopf Aboul-fetouh E. Mourad Peter G. Jones
author_sort	Henning Hopf
title	A surprising new route to 4-nitro-3-phenylisoxazole
title_short	A surprising new route to 4-nitro-3-phenylisoxazole
title_full	A surprising new route to 4-nitro-3-phenylisoxazole
title_fullStr	A surprising new route to 4-nitro-3-phenylisoxazole
title_full_unstemmed	A surprising new route to 4-nitro-3-phenylisoxazole
title_sort	surprising new route to 4-nitro-3-phenylisoxazole
publisher	Beilstein-Institut
series	Beilstein Journal of Organic Chemistry
issn	1860-5397
publishDate	2010-06-01
description	A one-pot synthesis of 4-nitro-3-phenylisoxazole has been carried out by treatment of cinnamyl alcohol dissolved in acetic acid with sodium nitrite; in addition, 4-phenyl-3-furoxanmethanol was obtained in 40% yield.
topic	cinnamyl alcohol furoxan derivatives isoxazole derivatives X-ray diffraction
url	https://doi.org/10.3762/bjoc.6.68
work_keys_str_mv	AT henninghopf asurprisingnewrouteto4nitro3phenylisoxazole AT aboulfetouhemourad asurprisingnewrouteto4nitro3phenylisoxazole AT petergjones asurprisingnewrouteto4nitro3phenylisoxazole AT henninghopf surprisingnewrouteto4nitro3phenylisoxazole AT aboulfetouhemourad surprisingnewrouteto4nitro3phenylisoxazole AT petergjones surprisingnewrouteto4nitro3phenylisoxazole
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A surprising new route to 4-nitro-3-phenylisoxazole

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