1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide

In the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480&#...

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Bibliographic Details
Main Authors: Hana Bashir Shawish, M. Jamil Maah, Seik Weng Ng
Format: Article
Language:English
Published: International Union of Crystallography 2010-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810014078
Description
Summary:In the title molecule, C10H13N3O3S, the thiosemicarbazide =N—NH—C(=S)—NH– fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)°]. A weak N—H...S hydrogen bond [3.480 (1) Å] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O—H...O and O—H...S hydrogen bonds generate a layer motif.
ISSN:1600-5368