Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure

Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure

Shuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as- synthesized BaMoO4 product was characterized by X-ray diffraction (X...

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Main Authors: Phuruangrat Anukorn, Kuntalue Budsabong, Thongtem Titipun, Thongtem Somchai
Format: Article
Language:English
Published: Sciendo 2015-09-01
Series:Materials Science-Poland
Subjects:
bamoo4
shuttle-like particles
luminescence
Online Access:https://doi.org/10.1515/msp-2015-0093
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spelling doaj-bb40979806574fdaa98f9385185948f22021-09-06T19:20:25ZengSciendoMaterials Science-Poland2083-134X2015-09-0133353754010.1515/msp-2015-0093msp-2015-0093Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructurePhuruangrat Anukorn0Kuntalue Budsabong1Thongtem Titipun2Thongtem Somchai3Department of Materials Science and Technology, Faculty of Science, Prince of Songkla University, Hat Yai, Songkhla 90112, ThailandElectron Microscopy Research and Service Center, Faculty of Science, Chiang Mai University, Chiang Mai 50200, ThailandDepartment of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai 50200, ThailandDepartment of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai 50200, ThailandShuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as- synthesized BaMoO4 product was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photolumines­cence (PL) spectroscopy. XRD patterns revealed that the products was tetragonal BaMoO4 phase. SEM and TEM characteriza­tion showed that the product had a shuttle-like BaMoO4 microstructure. PL of the shuttle-like BaMoO4 microstructure showed a maximum emission at 466 nm excited by 280 nm wavelength.https://doi.org/10.1515/msp-2015-0093bamoo4shuttle-like particlesluminescence
collection DOAJ
language English
format Article
sources DOAJ
author Phuruangrat Anukorn
Kuntalue Budsabong
Thongtem Titipun
Thongtem Somchai
spellingShingle Phuruangrat Anukorn
Kuntalue Budsabong
Thongtem Titipun
Thongtem Somchai
Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
Materials Science-Poland
bamoo4
shuttle-like particles
luminescence
author_facet Phuruangrat Anukorn
Kuntalue Budsabong
Thongtem Titipun
Thongtem Somchai
author_sort Phuruangrat Anukorn
title Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
title_short Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
title_full Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
title_fullStr Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
title_full_unstemmed Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO4 microstructure
title_sort microwave-assisted synthesis, characterization and photoluminescence of shuttle-like bamoo4 microstructure
publisher Sciendo
series Materials Science-Poland
issn 2083-134X
publishDate 2015-09-01
description Shuttle-like BaMoO4 microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as- synthesized BaMoO4 product was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photolumines­cence (PL) spectroscopy. XRD patterns revealed that the products was tetragonal BaMoO4 phase. SEM and TEM characteriza­tion showed that the product had a shuttle-like BaMoO4 microstructure. PL of the shuttle-like BaMoO4 microstructure showed a maximum emission at 466 nm excited by 280 nm wavelength.
topic bamoo4
shuttle-like particles
luminescence
url https://doi.org/10.1515/msp-2015-0093
work_keys_str_mv AT phuruangratanukorn microwaveassistedsynthesischaracterizationandphotoluminescenceofshuttlelikebamoo4microstructure
AT kuntaluebudsabong microwaveassistedsynthesischaracterizationandphotoluminescenceofshuttlelikebamoo4microstructure
AT thongtemtitipun microwaveassistedsynthesischaracterizationandphotoluminescenceofshuttlelikebamoo4microstructure
AT thongtemsomchai microwaveassistedsynthesischaracterizationandphotoluminescenceofshuttlelikebamoo4microstructure
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