Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process

Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process

The production of biodiesel using zeolite catalysts from geothermal solid waste has been studied. This study aims to make zeolite catalysts as catalysts in biodiesel production, assessing the effect of catalyst concentration, and temperature in the esterification–transesterification process on the b...

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Main Authors: Luqman Buchori, W. Widayat, Oki Muraza, Muhamad Iqbal Amali, Rahma Wulan Maulida, Jedy Prameswari
Format: Article
Language:English
Published: MDPI AG 2020-12-01
Series:Processes
Subjects:
analcime zeolite catalyst
biodiesel
geothermal solid waste
used cooking oil
yield of biodiesel
Online Access:https://www.mdpi.com/2227-9717/8/12/1629
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spelling doaj-b9ca6bc67f27481281a4b42595dc69372020-12-11T00:04:15ZengMDPI AGProcesses2227-97172020-12-0181629162910.3390/pr8121629Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification ProcessLuqman Buchori0W. Widayat1Oki Muraza2Muhamad Iqbal Amali3Rahma Wulan Maulida4Jedy Prameswari5Department of Chemical Engineering, Faculty of Engineering, Diponegoro University, Semarang 50275, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Diponegoro University, Semarang 50275, IndonesiaDepartment of Chemical Engineering & Center of Excellence in Nanotechnology (CENT), King Fahd University of Petroleum and Minerals (KFUPM), P.O. Box 5040, Dhahran 31261, Saudi ArabiaDepartment of Chemical Engineering, Faculty of Engineering, Diponegoro University, Semarang 50275, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Diponegoro University, Semarang 50275, IndonesiaDepartment of Chemical Engineering, Faculty of Engineering, Diponegoro University, Semarang 50275, IndonesiaThe production of biodiesel using zeolite catalysts from geothermal solid waste has been studied. This study aims to make zeolite catalysts as catalysts in biodiesel production, assessing the effect of catalyst concentration, and temperature in the esterification–transesterification process on the biodiesel yield produced. The results showed that the synthesized zeolite catalyst was an analcime zeolite catalyst (Al<sub>1.9</sub>Na<sub>1.86</sub>O<sub>12</sub>Si<sub>4</sub>). The biodiesel yield of 98.299% with 100% fatty acid alkyl ester (FAAE) content was achieved at a catalyst concentration of 5%wt and a reaction temperature of 300 °C for one-hour reaction time. The yield of biodiesel decreased with repeated catalysts, which experienced morphological changes before and after three usage times. Consequently, in this case, the catalyst cannot be regenerated.https://www.mdpi.com/2227-9717/8/12/1629analcime zeolite catalystbiodieselgeothermal solid wasteused cooking oilyield of biodiesel
collection DOAJ
language English
format Article
sources DOAJ
author Luqman Buchori
W. Widayat
Oki Muraza
Muhamad Iqbal Amali
Rahma Wulan Maulida
Jedy Prameswari
spellingShingle Luqman Buchori
W. Widayat
Oki Muraza
Muhamad Iqbal Amali
Rahma Wulan Maulida
Jedy Prameswari
Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
Processes
analcime zeolite catalyst
biodiesel
geothermal solid waste
used cooking oil
yield of biodiesel
author_facet Luqman Buchori
W. Widayat
Oki Muraza
Muhamad Iqbal Amali
Rahma Wulan Maulida
Jedy Prameswari
author_sort Luqman Buchori
title Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
title_short Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
title_full Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
title_fullStr Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
title_full_unstemmed Effect of Temperature and Concentration of Zeolite Catalysts from Geothermal Solid Waste in Biodiesel Production from Used Cooking Oil by Esterification–Transesterification Process
title_sort effect of temperature and concentration of zeolite catalysts from geothermal solid waste in biodiesel production from used cooking oil by esterification–transesterification process
publisher MDPI AG
series Processes
issn 2227-9717
publishDate 2020-12-01
description The production of biodiesel using zeolite catalysts from geothermal solid waste has been studied. This study aims to make zeolite catalysts as catalysts in biodiesel production, assessing the effect of catalyst concentration, and temperature in the esterification–transesterification process on the biodiesel yield produced. The results showed that the synthesized zeolite catalyst was an analcime zeolite catalyst (Al<sub>1.9</sub>Na<sub>1.86</sub>O<sub>12</sub>Si<sub>4</sub>). The biodiesel yield of 98.299% with 100% fatty acid alkyl ester (FAAE) content was achieved at a catalyst concentration of 5%wt and a reaction temperature of 300 °C for one-hour reaction time. The yield of biodiesel decreased with repeated catalysts, which experienced morphological changes before and after three usage times. Consequently, in this case, the catalyst cannot be regenerated.
topic analcime zeolite catalyst
biodiesel
geothermal solid waste
used cooking oil
yield of biodiesel
url https://www.mdpi.com/2227-9717/8/12/1629
work_keys_str_mv AT luqmanbuchori effectoftemperatureandconcentrationofzeolitecatalystsfromgeothermalsolidwasteinbiodieselproductionfromusedcookingoilbyesterificationtransesterificationprocess
AT wwidayat effectoftemperatureandconcentrationofzeolitecatalystsfromgeothermalsolidwasteinbiodieselproductionfromusedcookingoilbyesterificationtransesterificationprocess
AT okimuraza effectoftemperatureandconcentrationofzeolitecatalystsfromgeothermalsolidwasteinbiodieselproductionfromusedcookingoilbyesterificationtransesterificationprocess
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