<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine

<i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridi...

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Main Authors: Dhafer S. Zinad, Dunya L. AL-Duhaidahaw, Ahmed Al-Amiery, Abdul Amir H. Kadhum
Format: Article
Language:English
Published: MDPI AG 2018-11-01
Series:Molbank
Subjects:
Online Access:https://www.mdpi.com/1422-8599/2018/4/M1030
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spelling doaj-b8bbf9e75d9043c1abd903d3f0ccacc32020-11-24T20:56:59ZengMDPI AGMolbank1422-85992018-11-0120184M103010.3390/M1030M1030<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamineDhafer S. Zinad0Dunya L. AL-Duhaidahaw1Ahmed Al-Amiery2Abdul Amir H. Kadhum3Applied Science Department, University of Technology, Baghdad 10001, IraqPharmaceutical Chemistry Department, College of Pharmacy, University of Kufa, AL-Najaf 31001, IraqEnergy and Renewable Energies Technology Center, University of Technology, Baghdad 10001, IraqDepartment of Chemical &amp; Process Engineering, Faculty of Engineering &amp; Built Environment, Universiti Kebangsaan Malaysia, Bangi, Selangor 43600, Malaysia<i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) (<sup>1</sup>H-NMR and <sup>13</sup>C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high- performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.https://www.mdpi.com/1422-8599/2018/4/M10304-phenylenediaminefluorescentbutanolbipyridineimidazole
collection DOAJ
language English
format Article
sources DOAJ
author Dhafer S. Zinad
Dunya L. AL-Duhaidahaw
Ahmed Al-Amiery
Abdul Amir H. Kadhum
spellingShingle Dhafer S. Zinad
Dunya L. AL-Duhaidahaw
Ahmed Al-Amiery
Abdul Amir H. Kadhum
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
Molbank
4-phenylenediamine
fluorescent
butanol
bipyridine
imidazole
author_facet Dhafer S. Zinad
Dunya L. AL-Duhaidahaw
Ahmed Al-Amiery
Abdul Amir H. Kadhum
author_sort Dhafer S. Zinad
title <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
title_short <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
title_full <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
title_fullStr <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
title_full_unstemmed <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
title_sort <em>n</em>-[4-(1-methyl-1<em>h</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
publisher MDPI AG
series Molbank
issn 1422-8599
publishDate 2018-11-01
description <i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) (<sup>1</sup>H-NMR and <sup>13</sup>C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high- performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.
topic 4-phenylenediamine
fluorescent
butanol
bipyridine
imidazole
url https://www.mdpi.com/1422-8599/2018/4/M1030
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