<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine
<i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridi...
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doaj-b8bbf9e75d9043c1abd903d3f0ccacc32020-11-24T20:56:59ZengMDPI AGMolbank1422-85992018-11-0120184M103010.3390/M1030M1030<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamineDhafer S. Zinad0Dunya L. AL-Duhaidahaw1Ahmed Al-Amiery2Abdul Amir H. Kadhum3Applied Science Department, University of Technology, Baghdad 10001, IraqPharmaceutical Chemistry Department, College of Pharmacy, University of Kufa, AL-Najaf 31001, IraqEnergy and Renewable Energies Technology Center, University of Technology, Baghdad 10001, IraqDepartment of Chemical & Process Engineering, Faculty of Engineering & Built Environment, Universiti Kebangsaan Malaysia, Bangi, Selangor 43600, Malaysia<i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) (<sup>1</sup>H-NMR and <sup>13</sup>C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high- performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis.https://www.mdpi.com/1422-8599/2018/4/M10304-phenylenediaminefluorescentbutanolbipyridineimidazole |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Dhafer S. Zinad Dunya L. AL-Duhaidahaw Ahmed Al-Amiery Abdul Amir H. Kadhum |
spellingShingle |
Dhafer S. Zinad Dunya L. AL-Duhaidahaw Ahmed Al-Amiery Abdul Amir H. Kadhum <em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine Molbank 4-phenylenediamine fluorescent butanol bipyridine imidazole |
author_facet |
Dhafer S. Zinad Dunya L. AL-Duhaidahaw Ahmed Al-Amiery Abdul Amir H. Kadhum |
author_sort |
Dhafer S. Zinad |
title |
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
title_short |
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
title_full |
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
title_fullStr |
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
title_full_unstemmed |
<em>N</em>-[4-(1-Methyl-1<em>H</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
title_sort |
<em>n</em>-[4-(1-methyl-1<em>h</em>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine |
publisher |
MDPI AG |
series |
Molbank |
issn |
1422-8599 |
publishDate |
2018-11-01 |
description |
<i>N</i>-[4-(1-Methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridin-2′-yl]benzene-1,4-diamine was synthesized with a good yield by the reaction of 2′-chloro-4-(1-methyl-1<i>H</i>-imidazol-2-yl)-2,4′-bipyridine with 4-phenylenediamine. The functionalization of the pyridine was accomplished by a nucleophilic aromatic substitution (SNAr) reaction that afforded the target compound. The synthesized compound was characterized by chemical analysis, which includes nuclear magnetic resonance (NMR) (<sup>1</sup>H-NMR and <sup>13</sup>C-NMR), Thin Layer Chromatography-Mass Spectrometry (TLC-MS), high- performance liquid chromatography (HPLC), Gas Chromatography-Mass Spectrometry (GC-MS), and elemental analysis. |
topic |
4-phenylenediamine fluorescent butanol bipyridine imidazole |
url |
https://www.mdpi.com/1422-8599/2018/4/M1030 |
work_keys_str_mv |
AT dhaferszinad emnem41methyl1emhemimidazol2yl24bipyridin2ylbenzene14diamine AT dunyalalduhaidahaw emnem41methyl1emhemimidazol2yl24bipyridin2ylbenzene14diamine AT ahmedalamiery emnem41methyl1emhemimidazol2yl24bipyridin2ylbenzene14diamine AT abdulamirhkadhum emnem41methyl1emhemimidazol2yl24bipyridin2ylbenzene14diamine |
_version_ |
1716789150693195776 |