P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide

P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide

The title compound, C24H30N2P2S2, was obtained by the reaction of Ph2PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N—H...S hydrogen bonding influences the molecular conformation; a P—N—P—N tors...

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Main Authors: Anke Spannenberg, Anina Wöhl, Bhaskar R. Aluri, Normen Peulecke, Mohammed H. Al-Hazmi
Format: Article
Language:English
Published: International Union of Crystallography 2009-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809014238
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spelling doaj-b796bfeb1180440786d6e8bfbb1381a32020-11-25T02:46:52ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-05-01655o1084o108410.1107/S1600536809014238P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amideAnke SpannenbergAnina WöhlBhaskar R. AluriNormen PeuleckeMohammed H. Al-HazmiThe title compound, C24H30N2P2S2, was obtained by the reaction of Ph2PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N—H...S hydrogen bonding influences the molecular conformation; a P—N—P—N torsion angle of 2.28 (9)° is observed. The two phenyl rings attached to one P atom form a dihedral angle of 74.02 (4)°. http://scripts.iucr.org/cgi-bin/paper?S1600536809014238
collection DOAJ
language English
format Article
sources DOAJ
author Anke Spannenberg
Anina Wöhl
Bhaskar R. Aluri
Normen Peulecke
Mohammed H. Al-Hazmi
spellingShingle Anke Spannenberg
Anina Wöhl
Bhaskar R. Aluri
Normen Peulecke
Mohammed H. Al-Hazmi
P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
Acta Crystallographica Section E
author_facet Anke Spannenberg
Anina Wöhl
Bhaskar R. Aluri
Normen Peulecke
Mohammed H. Al-Hazmi
author_sort Anke Spannenberg
title P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
title_short P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
title_full P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
title_fullStr P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
title_full_unstemmed P-[N-(Diphenylphosphorothioyl)isopropylamino]-N-isopropyl-P-phenylthiophosphinic amide
title_sort p-[n-(diphenylphosphorothioyl)isopropylamino]-n-isopropyl-p-phenylthiophosphinic amide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-05-01
description The title compound, C24H30N2P2S2, was obtained by the reaction of Ph2PN(iPr)P(Ph)N(iPr)H with elemental sulfur in tetrahydrofuran. In the solid state, intramolecular N—H...S hydrogen bonding influences the molecular conformation; a P—N—P—N torsion angle of 2.28 (9)° is observed. The two phenyl rings attached to one P atom form a dihedral angle of 74.02 (4)°.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809014238
work_keys_str_mv AT ankespannenberg pndiphenylphosphorothioylisopropylaminonisopropylpphenylthiophosphinicamide
AT aninawamp246hl pndiphenylphosphorothioylisopropylaminonisopropylpphenylthiophosphinicamide
AT bhaskarraluri pndiphenylphosphorothioylisopropylaminonisopropylpphenylthiophosphinicamide
AT normenpeulecke pndiphenylphosphorothioylisopropylaminonisopropylpphenylthiophosphinicamide
AT mohammedhalhazmi pndiphenylphosphorothioylisopropylaminonisopropylpphenylthiophosphinicamide
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