The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate

The Synthesis and Molecular Structure of 1-(3,4-Dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1H)-one Hydrochloride Methanol Solvate

A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic...

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Bibliographic Details
Main Authors: Andreas Decken, Christopher M. Vogels, L. Ross C. Barclay, Kate J. Sullivan, Dylan T. McLaughlin, Raymond Roy, Steven R. Hall, Stephen A. Westcott
Format: Article
Language:English
Published: MDPI AG 2013-05-01
Series:Crystals
Subjects:
dopamine
hydroxypyridinone
ligand
X-ray
Online Access:http://www.mdpi.com/2073-4352/3/2/333
Description
Summary:A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.
ISSN:2073-4352

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