5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide

5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide

The asymmetric unit of the title compound C25H19N5OS, contains two molecules, A and B. In molecule A, the dihedral angles between the pyrazole ring and the C-bound phenyl group, the N-bound phenyl group and the thiadiazole ring are 32.30 (14), 52.25 (14) and 34.94 (12)&...

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Main Authors: K. Palani, K. B. Umesha, N. Srikantamurthy, S. S. Mahesh, Chandra, M. Mahendra
Format: Article
Language:English
Published: International Union of Crystallography 2013-12-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536813028766
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spelling doaj-b13f1233d243431880e19cff343393492020-11-24T22:08:23ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682013-12-016912o1736o173610.1107/S16005368130287665-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamideK. PalaniK. B. UmeshaN. SrikantamurthyS. S. MaheshChandraM. MahendraThe asymmetric unit of the title compound C25H19N5OS, contains two molecules, A and B. In molecule A, the dihedral angles between the pyrazole ring and the C-bound phenyl group, the N-bound phenyl group and the thiadiazole ring are 32.30 (14), 52.25 (14) and 34.94 (12)°, respectively. The corresponding angles in molecule B are 33.32 (14), 50.67 (15), and 70.30 (12)°, respectively. In the crystal, the A and B molecules are linked by pairs of N—H...N hydrogen bonds, generating R22(8) loops. This dimer linkage is reinforced by two C—H...O hydrogen bonds and one C—H...N hydrogen bond.http://scripts.iucr.org/cgi-bin/paper?S1600536813028766
collection DOAJ
language English
format Article
sources DOAJ
author K. Palani
K. B. Umesha
N. Srikantamurthy
S. S. Mahesh
Chandra
M. Mahendra
spellingShingle K. Palani
K. B. Umesha
N. Srikantamurthy
S. S. Mahesh
Chandra
M. Mahendra
5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
Acta Crystallographica Section E
author_facet K. Palani
K. B. Umesha
N. Srikantamurthy
S. S. Mahesh
Chandra
M. Mahendra
author_sort K. Palani
title 5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
title_short 5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
title_full 5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
title_fullStr 5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
title_full_unstemmed 5-Methyl-1,3-diphenyl-N-(5-phenyl-1,3,4-thiadiazol-2-yl)-1H-pyrazole-4-carboxamide
title_sort 5-methyl-1,3-diphenyl-n-(5-phenyl-1,3,4-thiadiazol-2-yl)-1h-pyrazole-4-carboxamide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2013-12-01
description The asymmetric unit of the title compound C25H19N5OS, contains two molecules, A and B. In molecule A, the dihedral angles between the pyrazole ring and the C-bound phenyl group, the N-bound phenyl group and the thiadiazole ring are 32.30 (14), 52.25 (14) and 34.94 (12)°, respectively. The corresponding angles in molecule B are 33.32 (14), 50.67 (15), and 70.30 (12)°, respectively. In the crystal, the A and B molecules are linked by pairs of N—H...N hydrogen bonds, generating R22(8) loops. This dimer linkage is reinforced by two C—H...O hydrogen bonds and one C—H...N hydrogen bond.
url http://scripts.iucr.org/cgi-bin/paper?S1600536813028766
work_keys_str_mv AT kpalani 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
AT kbumesha 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
AT nsrikantamurthy 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
AT ssmahesh 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
AT chandra 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
AT mmahendra 5methyl13diphenyln5phenyl134thiadiazol2yl1hpyrazole4carboxamide
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