Redetermination of catena-poly[[chloridolead(II)]-μ2-chlorido-di-μ2-thiourea-κ4S:S] at 100 K

Redetermination of catena-poly[[chloridolead(II)]-μ2-chlorido-di-μ2-thiourea-κ4S:S] at 100 K

Although the structure rerefinement (CCD data at 100 K) of the polymeric lead(II) thiourea complex, [PbCl2·2tu]n where (tu = SCN2H4), basically confirmed the previous study based on integrated Weissenberg data recorded at room temperature [Nardelli & Fava (1959). Acta Cryst. 12, 727–732]; all at...

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Bibliographic Details
Main Authors: Hafid Zouihri, Khalid Yamni, Youssef Messouss, Najib Tijani, Lahcen Messaoudi
Format: Article
Language:English
Published: International Union of Crystallography 2016-11-01
Series:IUCrData
Subjects:
crystal structure
redetermination
polymeric lead thiourea salt
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314616017454
Description
Summary:Although the structure rerefinement (CCD data at 100 K) of the polymeric lead(II) thiourea complex, [PbCl2·2tu]n where (tu = SCN2H4), basically confirmed the previous study based on integrated Weissenberg data recorded at room temperature [Nardelli & Fava (1959). Acta Cryst. 12, 727–732]; all atomic positions could be determined with significantly higher precision and accuracy. In addition, all H atoms could be located from difference maps, revealing details of the hydrogen-bonding scheme.
ISSN:2414-3146

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