Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior

Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior

In this work, the cocrystals of betulin with suberic acid were prepared by liquid-assisted grinding method using solvents of different polarity. The formation of cocrystals was confirmed by means of powder X-ray diffraction, IR spectroscopy and thermal analysis. It was shown that under heating, a st...

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Main Authors: Mikhailovskaya Anastasiya, Myz Svetlana, Gerasimov Konstantin, Kuznetsova Svetlana, Shakhtshneider Tatyana
Format: Article
Language:English
Published: EDP Sciences 2021-01-01
Series:MATEC Web of Conferences
Online Access:https://www.matec-conferences.org/articles/matecconf/pdf/2021/09/matecconf_rkfm2021_01019.pdf
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spelling doaj-abab11c2eb624d0dbf6a49137f4b4ae72021-07-09T11:41:19ZengEDP SciencesMATEC Web of Conferences2261-236X2021-01-013400101910.1051/matecconf/202134001019matecconf_rkfm2021_01019Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behaviorMikhailovskaya Anastasiya0Myz Svetlana1Gerasimov Konstantin2Kuznetsova Svetlana3Shakhtshneider Tatyana4Institute of Solid State Chemistry and Mechanochemistry SBRASInstitute of Solid State Chemistry and Mechanochemistry SBRASInstitute of Solid State Chemistry and Mechanochemistry SBRASInstitute of Chemistry and Chemical Technology, FRC KSCSB RASInstitute of Solid State Chemistry and Mechanochemistry SBRASIn this work, the cocrystals of betulin with suberic acid were prepared by liquid-assisted grinding method using solvents of different polarity. The formation of cocrystals was confirmed by means of powder X-ray diffraction, IR spectroscopy and thermal analysis. It was shown that under heating, a structural transformation occurred after water removal, followed by cocrystal dissociation.https://www.matec-conferences.org/articles/matecconf/pdf/2021/09/matecconf_rkfm2021_01019.pdf
collection DOAJ
language English
format Article
sources DOAJ
author Mikhailovskaya Anastasiya
Myz Svetlana
Gerasimov Konstantin
Kuznetsova Svetlana
Shakhtshneider Tatyana
spellingShingle Mikhailovskaya Anastasiya
Myz Svetlana
Gerasimov Konstantin
Kuznetsova Svetlana
Shakhtshneider Tatyana
Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
MATEC Web of Conferences
author_facet Mikhailovskaya Anastasiya
Myz Svetlana
Gerasimov Konstantin
Kuznetsova Svetlana
Shakhtshneider Tatyana
author_sort Mikhailovskaya Anastasiya
title Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
title_short Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
title_full Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
title_fullStr Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
title_full_unstemmed Сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
title_sort сocrystals of betulin with suberic acid: mechanochemical synthesis and thermal behavior
publisher EDP Sciences
series MATEC Web of Conferences
issn 2261-236X
publishDate 2021-01-01
description In this work, the cocrystals of betulin with suberic acid were prepared by liquid-assisted grinding method using solvents of different polarity. The formation of cocrystals was confirmed by means of powder X-ray diffraction, IR spectroscopy and thermal analysis. It was shown that under heating, a structural transformation occurred after water removal, followed by cocrystal dissociation.
url https://www.matec-conferences.org/articles/matecconf/pdf/2021/09/matecconf_rkfm2021_01019.pdf
work_keys_str_mv AT mikhailovskayaanastasiya socrystalsofbetulinwithsubericacidmechanochemicalsynthesisandthermalbehavior
AT myzsvetlana socrystalsofbetulinwithsubericacidmechanochemicalsynthesisandthermalbehavior
AT gerasimovkonstantin socrystalsofbetulinwithsubericacidmechanochemicalsynthesisandthermalbehavior
AT kuznetsovasvetlana socrystalsofbetulinwithsubericacidmechanochemicalsynthesisandthermalbehavior
AT shakhtshneidertatyana socrystalsofbetulinwithsubericacidmechanochemicalsynthesisandthermalbehavior
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