Synthesis of Isotope labeled Trichlorfon-methoxyl-D6 and Dichlorophos-methoxyl-D6

Synthesis of Isotope labeled Trichlorfon-methoxyl-D6 and Dichlorophos-methoxyl-D6

The efficient synthesis of two labeled standards trichlorfon-methoxyl-D6 and dichlorophos- methoxyl-D6 with CD3OD as the precursor were presented. Esterification of phosphorus trichloride with CD3OD provided dimethyl phosphate-methoxyl-D6, which was used to condense with trichloroaldehyde to give tr...

Full description

Bibliographic Details
Main Author:	YANG Wei-cheng1;LV Jing1;QI Qing-rui2;SHENG Li-yan1;LI Mei-hua1;YANG Chao1;LUO Yong1
Format:	Article
Language:	zho
Published:	Editorial Board of Journal of Isotopes 2014-02-01
Series:	Journal of Isotopes
Subjects:	isotope labeled synthesis dimethyl phosphate trichlorfon dichlorophos characterization
Online Access:	http://www.tws.org.cn/CN/10.7538/tws.2014.27.01.0008

Similar Items

Syntheses of Labeled Dimethyl Phthalate-D6
by: XU Zhong-jie;LU Wei-jing;SUN Wen;JIANG Zhe;LI Bing-yao;PAN Jie
Published: (2014-02-01)

Histopathologic changes in the kidney tissue of Prochilodus lineatus Valenciennes, 1836 (Characiformes, Prochilodontidae) induced by sublethal concentration of Trichlorfon exposure
by: Marcelo Leite da Veiga, et al.
Published: (2002-06-01)

Tissue Metabolism, Hematotoxicity, and Hepatotoxicity of Trichlorfon in Carassius auratus gibelio After a Single Oral Administration
by: Jianfei Lu, et al.
Published: (2018-05-01)

Lesões histopatológicas em fígado de <em>Prochilodus lineatus</em> (Pisces, Prochilodontidae) exposto à concetração subletal do inseticida organofosforado Dipterex 500® (Trichlorfon) Histopathologic lesions in the liver of <em>Prochilodus lineatus</em> (Pisces, Prochilodontidae) exposed to a sublethal concentration of the organophosphate insecticide Dipterex 500 ®(Trichlorfon)
by: Marcelo Leite da Veiga, et al.
Published: (2001-05-01)

Stable Isotope Compositions of Wild and Farmed S. Paramoamosion and its Implication for Tracebility
by: GUO Jie-min1,2;LIN Guang-hui1,3
Published: (2014-02-01)

Application of Stable Carbon Isotope Technique in the Research of Soil Rhizosphere Priming Effect
by: YUAN Hongzhao1;WANG Jiurong1;LIU Shoulong1;ZHU Zhenke1;GE Tida1;CHEN Shan1,2;WU Jinshui1
Published: (2018-02-01)

LC-MS Quantification of Site-Specific Phosphorylation Degree by Stable-Isotope Dimethyl Labeling Coupled with Phosphatase Dephosphorylation
by: Sin-Hong Chen, et al.
Published: (2020-11-01)

Syntheses of Stable Isotope Labeled D12-Malachite Green
by: YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
Published: (2014-02-01)

Identification of glycoproteins in mucous cells of the gill epithelium of Colossoma macropomum after exposure to organophosphate
by: S.E. Moron, et al.

Syntheses of Stable Isotopelabeled 1-(3-Methoxy-Phenyl)-［4-(4-Fluoro-2-Methoxy-D3-Phenylaminemethyl］-1h-［1,2,3］Triazole
by: XU Zhongjie1,2;TU Yahui1,2;ZHONG Jiaqi1,2;SUN Wen1,2;WANG Zhonghua3;WANG Haoran1,2;BAI Shaofei1,2;WU Fanhong3
Published: (2020-12-01)

Novel Hydrophobic Pt/Inorganic Catalyst Used in Hydrogen Isotope Exchange Reaction
by: JIA Qing-qing1;HU Shi-lin1;FENG Xiao-yan2;LIU Ya-ming1
Published: (2016-11-01)

Sulfur Isotope of Epilithic Mosses to Trace Variation of Atmospheric Sulfur Sources
by: HU Fei-fei1,2;PAN Jia-yong1,3;ZHANG Liang1,2;XIE Shu-rong3;CHEN Yi-ping3;XIA Fei1,3
Published: (2016-08-01)

Feasibility of Utilizing Stable-Isotope Dimethyl Labeling in Liquid Chromatography–Tandem Mass Spectrometry-Based Determination for Food Allergens—Case of Kiwifruit
by: Yi-Chen Shih, et al.
Published: (2019-05-01)

Anodic methoxylation of cinnamate esters
by: Pardini Vera L., et al.
Published: (2001-01-01)

Studies on low methoxyl pectins
by: Padival, Rajni A
Published: (2007)

The metathetical reactions of methoxyl radicals
by: Shaw, Robert
Published: (1959)

Methoxyl-substituted carbonium ions
by: Alfaro, J.
Published: (1972)

Central energy metabolism remains robust in acute steatotic hepatocytes challenged by a high free fatty acid load
by: Jens Niklas1,*, Anne Bonin1, Stefanie Mangin1, Joachim Bucher1, Stephanie Kopacz2, Madlen Matz-Soja 3, Carlo Thiel3, Rolf Gebhardt3, Ute Hofmann2 & Klaus Mauch1
Published: (2012-07-01)

Syntheses of Stable Isotope ［13C］/D Labelled p-Methoxybenzoic Acid
by: WANG Wei;DU Xiaoning;XU Jianfei;LEI Wen
Published: (2020-12-01)

Comparative Profiling of Triple-Negative Breast Carcinomas Tissue Glycoproteome by Sequential Purification of Glycoproteins and Stable Isotope Labeling
by: Xiang Chen, et al.
Published: (2016-01-01)

Discuss on Origin of Mineralizer CO2 from the Deep Seated Orebodies of Mianhuakeng Uranium Deposit in Northern Guangdong, China
by: PAN Chun-rong1,2;YANG Hai-lin2;PAN Jia-yong1
Published: (2017-04-01)

Toxicidade Aguda do Triclorfom em pacus juvenis (Piaractus mesopotamicus Holmberg, 1887)
by: Mataqueiro, Maria Isabel [UNESP]
Published: (2014)

Studies on some methoxyl- substituted carbonium ions
by: Ashton, W. R.
Published: (1970)

Methoxyl-Substituted Bridged Bicyclic Carbonium Ions
by: McManus, L. D.
Published: (1975)

The lignin and methoxyl content of some common crops.
by: Hurdis, John Wendell
Published: (1940)

Part I, Synthetic and mechanistic aspects of the anodic methoxylation reaction of methoxylated naphthalenes ; Part II, Directed monohydrolyses of quinone bisketals /
by: Dolson, Mark Glen
Published: (1981)

Isotopically Dimethyl Labeling-Based Quantitative Proteomic Analysis of Phosphoproteomes of Soybean Cultivars
by: Atieh Moradi, et al.
Published: (2021-08-01)

Strategies for Extending Metabolomics Studies with Stable Isotope Labelling and Fluxomics
by: Anubhav Srivastava, et al.
Published: (2016-10-01)

Preparation of 18F-Labeled Styryl Nitrogenous Heterocycles
by: LIU Yinli1;LI Zhongyong1,2
Published: (2018-02-01)

Simplified Synthesis of Isotopically Labeled 5,5-Dimethyl-pyrroline N-Oxide
by: Ronald P. Mason, et al.
Published: (2011-10-01)

Study on Enzymatic Activity of Pectinase for Degrading Methoxyl-Pectin
by: TSAI PEI CHEN, et al.
Published: (2006)

Effects of the Gelling Conditions on the Gelation of Low Methoxyl Pectin
by: Shien-Min Cheng, et al.
Published: (2001)

Analytical Considerations of Stable Isotope Labelling in Lipidomics
by: Alexander Triebl, et al.
Published: (2018-11-01)

Coupling Reaction of Oligo p-Phenylene Ethynylene and Peptide Antagonist RM26 Labeling with 131
by: JIAN Yuan1,2;ZHOU Zhi-jun2;ZHUO Lian-gang2;ZHAO Peng2;LIAO Wei2;WANG Guan-quan2;LIU Ning1
Published: (2016-08-01)

Multi-Residue Screening of Pesticides in Aquaculture Waters through Ultra-High-Performance Liquid Chromatograph-Q/Orbitrap Mass Spectrometry
by: Shou-Ying Wang, et al.
Published: (2020-04-01)

BIOADSORPSI Hg(II) OLEH PATI SAGU TAUT SILANG FOSFAT [Bioadsorption of Hg(II) by Crosslinked Sago Starch Phosphate]
by: Sri Sugiarti2), et al.
Published: (2012-12-01)

Exploratory Study on the Foliar Incorporation and Stability of Isotopically Labeled Amino Acids Applied to Turfgrass
by: Rachel M. McCoy, et al.
Published: (2020-03-01)

Herpetopanone, a diterpene from Herpetosiphon aurantiacus discovered by isotope labeling
by: Xinli Pan, et al.
Published: (2017-11-01)

Effect of the modified high methoxyl pectin on the stability of the fermented milk beverage
by: Yanhua Li, et al.
Published: (2018-01-01)

Preparation and Preliminary Biological Evaluation of 177Lu Labelled Rituximab
by: MA Xiu-feng1;ZHANG Jun-li2;LI Hong-yu1,2;LIANG Ji-xin1;YANG Yun2;YANG Chun-hui2;DU Jin1,3
Published: (2014-02-01)