Synthesis of Isotope labeled Trichlorfon-methoxyl-D6 and Dichlorophos-methoxyl-D6

The efficient synthesis of two labeled standards trichlorfon-methoxyl-D6 and dichlorophos- methoxyl-D6 with CD3OD as the precursor were presented. Esterification of phosphorus trichloride with CD3OD provided dimethyl phosphate-methoxyl-D6, which was used to condense with trichloroaldehyde to give tr...

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Bibliographic Details
Main Author: YANG Wei-cheng1;LV Jing1;QI Qing-rui2;SHENG Li-yan1;LI Mei-hua1;YANG Chao1;LUO Yong1
Format: Article
Language:zho
Published: Editorial Board of Journal of Isotopes 2014-02-01
Series:Journal of Isotopes
Subjects:
Online Access:http://www.tws.org.cn/CN/10.7538/tws.2014.27.01.0008