Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
The SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the...
Main Authors: | , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Hindawi Limited
2012-01-01
|
Series: | Journal of Nanomaterials |
Online Access: | http://dx.doi.org/10.1155/2012/861591 |
id |
doaj-a6929dcf7c464e079c471a268f52f431 |
---|---|
record_format |
Article |
spelling |
doaj-a6929dcf7c464e079c471a268f52f4312020-11-24T23:41:36ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292012-01-01201210.1155/2012/861591861591Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet ImpregnationSreejarani K. Pillai0Sarah C. Motshekga1Suprakas Sinha Ray2John Kennedy3DST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaDST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaDST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaNational Isotope Centre, GNS Science, 30 Gracefield Road, Lower Hutt 5010, New ZealandThe SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the results from X-ray diffraction. Enhanced field emission performance was observed for SnO2/CNTs composite prepared by a microwave method when compared to pure CNTs and SnO2/CNTs composite prepared by conventional wet impregnation. The dependence of emission current density on the electric field followed a Fowler-Nordheim relationship.http://dx.doi.org/10.1155/2012/861591 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Sreejarani K. Pillai Sarah C. Motshekga Suprakas Sinha Ray John Kennedy |
spellingShingle |
Sreejarani K. Pillai Sarah C. Motshekga Suprakas Sinha Ray John Kennedy Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation Journal of Nanomaterials |
author_facet |
Sreejarani K. Pillai Sarah C. Motshekga Suprakas Sinha Ray John Kennedy |
author_sort |
Sreejarani K. Pillai |
title |
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation |
title_short |
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation |
title_full |
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation |
title_fullStr |
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation |
title_full_unstemmed |
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation |
title_sort |
field emission characteristics of sno2/cnts composites prepared by microwave-assisted wet impregnation |
publisher |
Hindawi Limited |
series |
Journal of Nanomaterials |
issn |
1687-4110 1687-4129 |
publishDate |
2012-01-01 |
description |
The SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the results from X-ray diffraction. Enhanced field emission performance was observed for SnO2/CNTs composite prepared by a microwave method when compared to pure CNTs and SnO2/CNTs composite prepared by conventional wet impregnation. The dependence of emission current density on the electric field followed a Fowler-Nordheim relationship. |
url |
http://dx.doi.org/10.1155/2012/861591 |
work_keys_str_mv |
AT sreejaranikpillai fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation AT sarahcmotshekga fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation AT suprakassinharay fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation AT johnkennedy fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation |
_version_ |
1725506420378435584 |