Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation

The SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the...

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Main Authors: Sreejarani K. Pillai, Sarah C. Motshekga, Suprakas Sinha Ray, John Kennedy
Format: Article
Language:English
Published: Hindawi Limited 2012-01-01
Series:Journal of Nanomaterials
Online Access:http://dx.doi.org/10.1155/2012/861591
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spelling doaj-a6929dcf7c464e079c471a268f52f4312020-11-24T23:41:36ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292012-01-01201210.1155/2012/861591861591Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet ImpregnationSreejarani K. Pillai0Sarah C. Motshekga1Suprakas Sinha Ray2John Kennedy3DST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaDST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaDST/CSIR Nanotechnology Innovation Centre, National Centre for Nano-Structured Materials, Council for Scientific and Industrial Research, Pretoria 0001, South AfricaNational Isotope Centre, GNS Science, 30 Gracefield Road, Lower Hutt 5010, New ZealandThe SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the results from X-ray diffraction. Enhanced field emission performance was observed for SnO2/CNTs composite prepared by a microwave method when compared to pure CNTs and SnO2/CNTs composite prepared by conventional wet impregnation. The dependence of emission current density on the electric field followed a Fowler-Nordheim relationship.http://dx.doi.org/10.1155/2012/861591
collection DOAJ
language English
format Article
sources DOAJ
author Sreejarani K. Pillai
Sarah C. Motshekga
Suprakas Sinha Ray
John Kennedy
spellingShingle Sreejarani K. Pillai
Sarah C. Motshekga
Suprakas Sinha Ray
John Kennedy
Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
Journal of Nanomaterials
author_facet Sreejarani K. Pillai
Sarah C. Motshekga
Suprakas Sinha Ray
John Kennedy
author_sort Sreejarani K. Pillai
title Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
title_short Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
title_full Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
title_fullStr Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
title_full_unstemmed Field Emission Characteristics of SnO2/CNTs Composites Prepared by Microwave-Assisted Wet Impregnation
title_sort field emission characteristics of sno2/cnts composites prepared by microwave-assisted wet impregnation
publisher Hindawi Limited
series Journal of Nanomaterials
issn 1687-4110
1687-4129
publishDate 2012-01-01
description The SnO2/CNT composites were prepared by microwave-assisted wet impregnation at 60°C. The process was optimized by varying the microwave power and reaction time. Raman analysis showed the typical features of the rutile phase of as-synthesized SnO2 nanoparticles on CNTs, which was consistent with the results from X-ray diffraction. Enhanced field emission performance was observed for SnO2/CNTs composite prepared by a microwave method when compared to pure CNTs and SnO2/CNTs composite prepared by conventional wet impregnation. The dependence of emission current density on the electric field followed a Fowler-Nordheim relationship.
url http://dx.doi.org/10.1155/2012/861591
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AT suprakassinharay fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation
AT johnkennedy fieldemissioncharacteristicsofsno2cntscompositespreparedbymicrowaveassistedwetimpregnation
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