Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
In this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3&...
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doaj-a0e0aa60fd694fb1aab52659176e23f92020-11-24T21:17:44ZengMDPI AGSensors1424-82202019-03-01195125710.3390/s19051257s19051257Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene SensorXiaofei Liu0Xintai Su1Chao Yang2Kongjun Ma3Ministry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaThe Key Laboratory of Pollution Control and Ecosystem Restoration in Industry Clusters (Ministry of Education), School of Environment and Energy, South China University of Technology, Guangzhou 510006, ChinaMinistry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaMinistry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaIn this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3·0.33H2O, which were mainly composed of nanorods with different crystal planes. The sensing performance of WO3·0.33H2O nanorod bundles prepared by the addition of PABA (100 ppm cyclohexene, Ra/Rg = 50.6) was found to be better than the WO3 synthesized without PABA (100 ppm cyclohexene, Ra/Rg = 1.3) for the detection of cyclohexene. The new synthesis route and sensing characteristics of as-synthesized WO3·0.33H2O nanorods revealed a promising candidate for the preparation of the cost-effective gas sensors.http://www.mdpi.com/1424-8220/19/5/1257hydrothermalWO3·0.33H2Op-aminobenzoic acidnanorod bundlescyclohexenegas sensing |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Xiaofei Liu Xintai Su Chao Yang Kongjun Ma |
spellingShingle |
Xiaofei Liu Xintai Su Chao Yang Kongjun Ma Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor Sensors hydrothermal WO3·0.33H2O p-aminobenzoic acid nanorod bundles cyclohexene gas sensing |
author_facet |
Xiaofei Liu Xintai Su Chao Yang Kongjun Ma |
author_sort |
Xiaofei Liu |
title |
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor |
title_short |
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor |
title_full |
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor |
title_fullStr |
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor |
title_full_unstemmed |
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor |
title_sort |
hydrothermal synthesis of wo3·0.33h2o nanorod bundles as a highly sensitive cyclohexene sensor |
publisher |
MDPI AG |
series |
Sensors |
issn |
1424-8220 |
publishDate |
2019-03-01 |
description |
In this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3·0.33H2O, which were mainly composed of nanorods with different crystal planes. The sensing performance of WO3·0.33H2O nanorod bundles prepared by the addition of PABA (100 ppm cyclohexene, Ra/Rg = 50.6) was found to be better than the WO3 synthesized without PABA (100 ppm cyclohexene, Ra/Rg = 1.3) for the detection of cyclohexene. The new synthesis route and sensing characteristics of as-synthesized WO3·0.33H2O nanorods revealed a promising candidate for the preparation of the cost-effective gas sensors. |
topic |
hydrothermal WO3·0.33H2O p-aminobenzoic acid nanorod bundles cyclohexene gas sensing |
url |
http://www.mdpi.com/1424-8220/19/5/1257 |
work_keys_str_mv |
AT xiaofeiliu hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor AT xintaisu hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor AT chaoyang hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor AT kongjunma hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor |
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1726012505272090624 |