Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor

In this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3&...

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Main Authors: Xiaofei Liu, Xintai Su, Chao Yang, Kongjun Ma
Format: Article
Language:English
Published: MDPI AG 2019-03-01
Series:Sensors
Subjects:
Online Access:http://www.mdpi.com/1424-8220/19/5/1257
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spelling doaj-a0e0aa60fd694fb1aab52659176e23f92020-11-24T21:17:44ZengMDPI AGSensors1424-82202019-03-01195125710.3390/s19051257s19051257Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene SensorXiaofei Liu0Xintai Su1Chao Yang2Kongjun Ma3Ministry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaThe Key Laboratory of Pollution Control and Ecosystem Restoration in Industry Clusters (Ministry of Education), School of Environment and Energy, South China University of Technology, Guangzhou 510006, ChinaMinistry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaMinistry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, ChinaIn this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3·0.33H2O, which were mainly composed of nanorods with different crystal planes. The sensing performance of WO3·0.33H2O nanorod bundles prepared by the addition of PABA (100 ppm cyclohexene, Ra/Rg = 50.6) was found to be better than the WO3 synthesized without PABA (100 ppm cyclohexene, Ra/Rg = 1.3) for the detection of cyclohexene. The new synthesis route and sensing characteristics of as-synthesized WO3·0.33H2O nanorods revealed a promising candidate for the preparation of the cost-effective gas sensors.http://www.mdpi.com/1424-8220/19/5/1257hydrothermalWO3·0.33H2Op-aminobenzoic acidnanorod bundlescyclohexenegas sensing
collection DOAJ
language English
format Article
sources DOAJ
author Xiaofei Liu
Xintai Su
Chao Yang
Kongjun Ma
spellingShingle Xiaofei Liu
Xintai Su
Chao Yang
Kongjun Ma
Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
Sensors
hydrothermal
WO3·0.33H2O
p-aminobenzoic acid
nanorod bundles
cyclohexene
gas sensing
author_facet Xiaofei Liu
Xintai Su
Chao Yang
Kongjun Ma
author_sort Xiaofei Liu
title Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
title_short Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
title_full Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
title_fullStr Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
title_full_unstemmed Hydrothermal Synthesis of WO3·0.33H2O Nanorod Bundles as a Highly Sensitive Cyclohexene Sensor
title_sort hydrothermal synthesis of wo3·0.33h2o nanorod bundles as a highly sensitive cyclohexene sensor
publisher MDPI AG
series Sensors
issn 1424-8220
publishDate 2019-03-01
description In this paper, WO3·0.33H2O nanorods were prepared through a simple hydrothermal method using p-aminobenzoic acid (PABA) as an auxiliary reagent. X-ray diffraction (XRD) and transmission electron microscopy (TEM) images showed that the products with PABA addition were orthorhombic WO3·0.33H2O, which were mainly composed of nanorods with different crystal planes. The sensing performance of WO3·0.33H2O nanorod bundles prepared by the addition of PABA (100 ppm cyclohexene, Ra/Rg = 50.6) was found to be better than the WO3 synthesized without PABA (100 ppm cyclohexene, Ra/Rg = 1.3) for the detection of cyclohexene. The new synthesis route and sensing characteristics of as-synthesized WO3·0.33H2O nanorods revealed a promising candidate for the preparation of the cost-effective gas sensors.
topic hydrothermal
WO3·0.33H2O
p-aminobenzoic acid
nanorod bundles
cyclohexene
gas sensing
url http://www.mdpi.com/1424-8220/19/5/1257
work_keys_str_mv AT xiaofeiliu hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor
AT xintaisu hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor
AT chaoyang hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor
AT kongjunma hydrothermalsynthesisofwo3033h2onanorodbundlesasahighlysensitivecyclohexenesensor
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