Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers

The aim of this study consisted in the development of an alternative synthesis procedure for hybrid ultrafiltration membranes for water purification. The membranes were obtained by wet-phase inversion method based on aliquots of polysulfone (PSF) and graphene nanoplatelets modified with poly(styrene...

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Main Authors: Alexandra Mocanu, Edina Rusen, Aurel Diacon, Celina Damian, Adrian Dinescu, Mirela Suchea
Format: Article
Language:English
Published: Hindawi Limited 2017-01-01
Series:Journal of Nanomaterials
Online Access:http://dx.doi.org/10.1155/2017/1401503
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spelling doaj-9f14e2178d644191be4962cfd87b065e2020-11-25T00:16:02ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292017-01-01201710.1155/2017/14015031401503Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble PolymersAlexandra Mocanu0Edina Rusen1Aurel Diacon2Celina Damian3Adrian Dinescu4Mirela Suchea5Department of Chemical and Biochemical Engineering, University Politehnica of Bucharest, 1-7 Gh. Polizu Street, 011061 Bucharest, RomaniaDepartment of Bioresources and Polymer Science, University Politehnica of Bucharest, 1-7 Gh. Polizu Street, 011061 Bucharest, RomaniaDepartment of Bioresources and Polymer Science, University Politehnica of Bucharest, 1-7 Gh. Polizu Street, 011061 Bucharest, RomaniaDepartment of Bioresources and Polymer Science, University Politehnica of Bucharest, 1-7 Gh. Polizu Street, 011061 Bucharest, RomaniaNational Institute for Research and Development in Microtechnologies (IMT-Bucharest), 126 A, Erou Iancu Nicolae Street, P.O. Box 38-160, 023573 Bucharest, RomaniaCenter of Materials Technology and Photonics, School of Engineering, Technological Educational Institute of Crete, 71004 Heraklion, GreeceThe aim of this study consisted in the development of an alternative synthesis procedure for hybrid ultrafiltration membranes for water purification. The membranes were obtained by wet-phase inversion method based on aliquots of polysulfone (PSF) and graphene nanoplatelets modified with poly(styrene) (G-PST). The hybrid materials were modified by electrochemical deposition of zinc oxide (ZnO) on one side of the membranes in the presence of water soluble polymers. Raman, XPS, and TGA analyses were used to characterize the chemical and thermal characteristics of the PST-G. SEM analysis showed the formation of asymmetric porous configuration in all cases and the generation of ZnO with different shapes/structures on the bottom surface of the membrane or inside the porous channels. EDS analysis confirmed the formation of ZnO.http://dx.doi.org/10.1155/2017/1401503
collection DOAJ
language English
format Article
sources DOAJ
author Alexandra Mocanu
Edina Rusen
Aurel Diacon
Celina Damian
Adrian Dinescu
Mirela Suchea
spellingShingle Alexandra Mocanu
Edina Rusen
Aurel Diacon
Celina Damian
Adrian Dinescu
Mirela Suchea
Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
Journal of Nanomaterials
author_facet Alexandra Mocanu
Edina Rusen
Aurel Diacon
Celina Damian
Adrian Dinescu
Mirela Suchea
author_sort Alexandra Mocanu
title Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
title_short Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
title_full Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
title_fullStr Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
title_full_unstemmed Electrochemical Deposition of Zinc Oxide on the Surface of Composite Membrane Polysulfone-Graphene-Polystyrene in the Presence of Water Soluble Polymers
title_sort electrochemical deposition of zinc oxide on the surface of composite membrane polysulfone-graphene-polystyrene in the presence of water soluble polymers
publisher Hindawi Limited
series Journal of Nanomaterials
issn 1687-4110
1687-4129
publishDate 2017-01-01
description The aim of this study consisted in the development of an alternative synthesis procedure for hybrid ultrafiltration membranes for water purification. The membranes were obtained by wet-phase inversion method based on aliquots of polysulfone (PSF) and graphene nanoplatelets modified with poly(styrene) (G-PST). The hybrid materials were modified by electrochemical deposition of zinc oxide (ZnO) on one side of the membranes in the presence of water soluble polymers. Raman, XPS, and TGA analyses were used to characterize the chemical and thermal characteristics of the PST-G. SEM analysis showed the formation of asymmetric porous configuration in all cases and the generation of ZnO with different shapes/structures on the bottom surface of the membrane or inside the porous channels. EDS analysis confirmed the formation of ZnO.
url http://dx.doi.org/10.1155/2017/1401503
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