Nonapiperidinium monohydrogen decavanadate tetranitrate

Nonapiperidinium monohydrogen decavanadate tetranitrate

The title compound, (C5H12N)9[HV10O28](NO3)4, contains a monoprotonated decavanadate polyanion which lies on an inversion center. All the piperidinium cations adopt chair conformations. In the crystal structure, intermolecular N—H...O hydrogen bonds form chains along [001]. As well as...

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Main Authors: Ahmed Driss, Regaya Ksiksi, Mohsen Graia
Format: Article
Language:English
Published: International Union of Crystallography 2009-08-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809026555
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spelling doaj-9b006a6d3d21427fb62f3df16ea528fe2020-11-24T21:30:37ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-08-01658m953m95410.1107/S1600536809026555Nonapiperidinium monohydrogen decavanadate tetranitrateAhmed DrissRegaya KsiksiMohsen GraiaThe title compound, (C5H12N)9[HV10O28](NO3)4, contains a monoprotonated decavanadate polyanion which lies on an inversion center. All the piperidinium cations adopt chair conformations. In the crystal structure, intermolecular N—H...O hydrogen bonds form chains along [001]. As well as half of a polyanion, the asymmetric unit contains one full and two half-occupancy nitrate ions and four full occupancy and one half-occupancy piperidinium cations; the half-occupancy piperidinium cation is disordered over two general sites with occupancies of 0.32 and 0.18, and is, in turn, disordered over an inversion center. http://scripts.iucr.org/cgi-bin/paper?S1600536809026555
collection DOAJ
language English
format Article
sources DOAJ
author Ahmed Driss
Regaya Ksiksi
Mohsen Graia
spellingShingle Ahmed Driss
Regaya Ksiksi
Mohsen Graia
Nonapiperidinium monohydrogen decavanadate tetranitrate
Acta Crystallographica Section E
author_facet Ahmed Driss
Regaya Ksiksi
Mohsen Graia
author_sort Ahmed Driss
title Nonapiperidinium monohydrogen decavanadate tetranitrate
title_short Nonapiperidinium monohydrogen decavanadate tetranitrate
title_full Nonapiperidinium monohydrogen decavanadate tetranitrate
title_fullStr Nonapiperidinium monohydrogen decavanadate tetranitrate
title_full_unstemmed Nonapiperidinium monohydrogen decavanadate tetranitrate
title_sort nonapiperidinium monohydrogen decavanadate tetranitrate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-08-01
description The title compound, (C5H12N)9[HV10O28](NO3)4, contains a monoprotonated decavanadate polyanion which lies on an inversion center. All the piperidinium cations adopt chair conformations. In the crystal structure, intermolecular N—H...O hydrogen bonds form chains along [001]. As well as half of a polyanion, the asymmetric unit contains one full and two half-occupancy nitrate ions and four full occupancy and one half-occupancy piperidinium cations; the half-occupancy piperidinium cation is disordered over two general sites with occupancies of 0.32 and 0.18, and is, in turn, disordered over an inversion center.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809026555
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AT regayaksiksi nonapiperidiniummonohydrogendecavanadatetetranitrate
AT mohsengraia nonapiperidiniummonohydrogendecavanadatetetranitrate
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