Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks
The present article describes an efficient one-pot method for the preparation of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-trione derivatives from a three-component condensation reaction of 1,3-indandione, aromatic amines and isatins in the presence of a zinc terephthalate metal-organic...
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Online Access: | http://dx.doi.org/10.1080/17518253.2018.1434565 |
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doaj-98955ed3a1fb4f9b88116f201d48125e2020-11-24T21:53:58ZengTaylor & Francis GroupGreen Chemistry Letters and Reviews1751-82531751-71922018-01-01111475310.1080/17518253.2018.14345651434565Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworksMohammad Ali Ghasemzadeh0Mohammad Hossein Abdollahi-Basir1Boshra Mirhosseini-Eshkevari2Islamic Azad UniversityIslamic Azad UniversityIslamic Azad UniversityThe present article describes an efficient one-pot method for the preparation of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-trione derivatives from a three-component condensation reaction of 1,3-indandione, aromatic amines and isatins in the presence of a zinc terephthalate metal-organic framework Zn (BDC) MOF as the catalyst under solvent-free conditions. High yields, short reaction times, simple workup and environmentally benign procedure are advantages of this protocol. The Zn (BDC) MOF catalyst can be recovered and reused several times without loss of activity. The catalyst was characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, Fourier transform infra red, X-ray powder diffraction and thermal gravimetric analysis.http://dx.doi.org/10.1080/17518253.2018.1434565Spiro compoundsZn (BDC)multi-component reactionsmetal-organic frameworkssolvent-free |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Mohammad Ali Ghasemzadeh Mohammad Hossein Abdollahi-Basir Boshra Mirhosseini-Eshkevari |
spellingShingle |
Mohammad Ali Ghasemzadeh Mohammad Hossein Abdollahi-Basir Boshra Mirhosseini-Eshkevari Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks Green Chemistry Letters and Reviews Spiro compounds Zn (BDC) multi-component reactions metal-organic frameworks solvent-free |
author_facet |
Mohammad Ali Ghasemzadeh Mohammad Hossein Abdollahi-Basir Boshra Mirhosseini-Eshkevari |
author_sort |
Mohammad Ali Ghasemzadeh |
title |
Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
title_short |
Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
title_full |
Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
title_fullStr |
Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
title_full_unstemmed |
Multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
title_sort |
multi-component synthesis of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-triones using zinc terephthalate metal-organic frameworks |
publisher |
Taylor & Francis Group |
series |
Green Chemistry Letters and Reviews |
issn |
1751-8253 1751-7192 |
publishDate |
2018-01-01 |
description |
The present article describes an efficient one-pot method for the preparation of spiro[diindeno[1,2-b:2′,1′-e]pyridine-11,3′-indoline]-trione derivatives from a three-component condensation reaction of 1,3-indandione, aromatic amines and isatins in the presence of a zinc terephthalate metal-organic framework Zn (BDC) MOF as the catalyst under solvent-free conditions. High yields, short reaction times, simple workup and environmentally benign procedure are advantages of this protocol. The Zn (BDC) MOF catalyst can be recovered and reused several times without loss of activity. The catalyst was characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, Fourier transform infra red, X-ray powder diffraction and thermal gravimetric analysis. |
topic |
Spiro compounds Zn (BDC) multi-component reactions metal-organic frameworks solvent-free |
url |
http://dx.doi.org/10.1080/17518253.2018.1434565 |
work_keys_str_mv |
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1725869800700248064 |