Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate

Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate

An improved crystal structure of the title compound, C14H12O8S4, is reported. The structure, previously solved using the heavy-atom method (R = 7.1%), has now been solved using direct methods. Due to the improved quality of the data set an R value of 2.06% could be achieved. In the crystal, C&am...

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Main Authors: Felix Katzsch, Edwin Weber
Format: Article
Language:English
Published: International Union of Crystallography 2012-08-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812029534
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spelling doaj-8ea36f1485f24b2a9ae8927ae4ba74652020-11-25T01:56:47ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-08-01688o2354o235510.1107/S1600536812029534Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylateFelix KatzschEdwin WeberAn improved crystal structure of the title compound, C14H12O8S4, is reported. The structure, previously solved using the heavy-atom method (R = 7.1%), has now been solved using direct methods. Due to the improved quality of the data set an R value of 2.06% could be achieved. In the crystal, C—H...S and C—H...O contacts link the molecules.http://scripts.iucr.org/cgi-bin/paper?S1600536812029534
collection DOAJ
language English
format Article
sources DOAJ
author Felix Katzsch
Edwin Weber
spellingShingle Felix Katzsch
Edwin Weber
Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
Acta Crystallographica Section E
author_facet Felix Katzsch
Edwin Weber
author_sort Felix Katzsch
title Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
title_short Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
title_full Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
title_fullStr Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
title_full_unstemmed Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
title_sort redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-08-01
description An improved crystal structure of the title compound, C14H12O8S4, is reported. The structure, previously solved using the heavy-atom method (R = 7.1%), has now been solved using direct methods. Due to the improved quality of the data set an R value of 2.06% could be achieved. In the crystal, C—H...S and C—H...O contacts link the molecules.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812029534
work_keys_str_mv AT felixkatzsch redeterminationoftetramethyltetrathiafulvalene2367tetracarboxylate
AT edwinweber redeterminationoftetramethyltetrathiafulvalene2367tetracarboxylate
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