Crystal structure of 4-(4-methoxyphenyl)-4′,4′-dimethyl-3-p-tolyl-3′,4′-dihydro-1′H,3H-spiro[isoxazole-5,2′-naphthalen]-1′-one

Crystal structure of 4-(4-methoxyphenyl)-4′,4′-dimethyl-3-p-tolyl-3′,4′-dihydro-1′H,3H-spiro[isoxazole-5,2′-naphthalen]-1′-one

In the title compound, C28H27NO3, the cyclohexanone and isoxazole rings have envelope conformations, with the methylene and spiro C atoms as the flaps, respectively. The mean plane of the isoxazole ring is inclined slightly to the p-tolyl ring, making a dihedral angle of 14.20 (9)°, and is nearly pe...

Full description

Bibliographic Details
Main Authors:	Mohamed Akhazzane, Ghali Al Houari, Mohamed El Yazidi, Mohamed Saadi, Lahcen El Ammari
Format:	Article
Language:	English
Published:	International Union of Crystallography 2015-12-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure isoxazole tetralone
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2056989015022033

Similar Items

2-Methyl-3′-(4-methylphenyl)-4′-(2-nitrophenyl)-4′H-spiro[chroman-3,5′-isoxazol]-4-one
by: Asmae Mahfoud, et al.
Published: (2018-07-01)

3′-(4-Chlorophenyl)-4′-phenyl-3H,4′H-spiro[benzo[b]thiophene-2,5′-isoxazol]-3-one
by: Mohamed Bakhouch, et al.
Published: (2017-05-01)

3′,4′-Diphenyl-3H,4′H-spiro[benzo[b]thiophene-2,5′-isoxazol]-3-one
by: Mohamed Bakhouch, et al.
Published: (2018-07-01)

Crystal structure of 3,4′-diphenyl-3′-p-tolyl-4′H-spiro[indan-2,5′-[1,2]oxazol]-1-one
by: Asmae Mahfoud, et al.
Published: (2015-11-01)

Crystal structure of (E)-4-ethyl-2-(4-methoxybenzylidene)-3,4-dihydronaphthalen-1(2H)-one
by: Mohamed Akhazzane, et al.
Published: (2015-06-01)

5-[5-(4-Chlorophenyl)isoxazol-3-yl]-N-phenyl-1,3,4-oxadiazol-2-amine
by: Gamal A. El-Hiti, et al.
Published: (2019-01-01)

3&#8242;-(4-Methoxyphenyl)-4&#8242;-phenyl-3H,4&#8242;H-spiro[1-benzothiophene-2,5&#8242;-isoxazol]-3-one
by: Adil Boughaleb, et al.
Published: (2011-07-01)

Crystal structure of 2-amino-3-cyano-4-(4-methoxyphenyl)-4H-1-benzothieno[3,2-b]pyran
by: Mohamed Bakhouch, et al.
Published: (2015-12-01)

Ethyl 2-amino-4-(3-nitrophenyl)-4H-1-benzothieno[3,2-b]pyran-3-carboxylate
by: Mohamed Bakhouch, et al.
Published: (2014-05-01)

Crystal structure of ethyl 2-amino-4-(4-methoxyphenyl)-4H-1-benzothieno[3,2-b]pyran-3-carboxylate
by: Mohamed Bakhouch, et al.
Published: (2015-05-01)

3-Difluoromethyl-5-[4-(trifluoromethyl)phenyl]isoxazole
by: Hui Zhao
Published: (2018-04-01)

Crystal structure and Hirshfeld surface analysis of (Z)-3-methyl-4-(thiophen-2-ylmethylidene)isoxazol-5(4H)-one
by: Rima Laroum, et al.
Published: (2021-04-01)

Crystal structures of methyl 3-(4-isopropylphenyl)-1-methyl-1,2,3,3a,4,9b-hexahydrothiochromeno[4,3-b]pyrrole-3a-carboxylate, methyl 1-methyl-3-(o-tolyl)-1,2,3,3a,4,9b-hexahydrothiochromeno[4,3-b]pyrrole-3a-carboxylate and methyl 1-methyl-3-(o-tolyl)-3,3a,4,9b-tetrahydro-1H-thiochromeno[4,3-c]isoxazole-3a-carboxylate
by: R. Raja, et al.
Published: (2015-06-01)

3-(4-Bromophenyl)-4-{[3-hydroxy-6-(hydroxymethyl)-4-oxo-4<i>H</i>-pyran-2-yl](<i>m</i>-tolyl)methyl}isoxazol-5(2<i>H</i>)-one
by: Yuliya E. Ryzhkova, et al.
Published: (2020-05-01)

(2RS,4&#8242;RS)-3&#8242;-(3-Chloro-4-methoxyphenyl)-4&#8242;-phenyl-4&#8242;H-spiro[indene-2,5&#8242;-isoxazol]-1(3H)-one ethanol monosolvate
by: Adil Boughaleb, et al.
Published: (2011-09-01)

4-tert-Butyl-3&#8242;,4&#8242;-bis(4-methylphenyl)-3,4-dihydro-1H,4&#8242;H-spiro[naphthalene-2,5&#8242;-[1,2]oxazol]-1-one
by: Mohamed Akhazzane, et al.
Published: (2011-07-01)

Crystal structure of (E)-2-(4-chlorobenzylidene)-3,4-dihydronaphthalen-1(2H)-one: a second monoclinic polymorph
by: Muhammad Haroon, et al.
Published: (2015-10-01)

Potassium phthalimide as efficient basic organocatalyst for the synthesis of 3,4-disubstituted isoxazol-5(4H)-ones in aqueous medium
by: Hamzeh Kiyani, et al.
Published: (2017-01-01)

5-(4-Methoxyphenyl)-4-methyl-1-phenyl-3-p-tolyl-1H-pyrazole
by: Yahya Ben Soumane, et al.
Published: (2017-11-01)

4-tert-Butyl-4&#8242;-(4-methoxyphenyl)-3&#8242;-(4-methylphenyl)-1,2,3,4-tetrahydrospiro[naphthalene-2,5&#8242;(4&#8242;H)-1,2-oxazol]-1-one
by: Mohamed Akhazzane, et al.
Published: (2010-11-01)

Crystal structure of 5-{3-[2,6-dimethyl-4-(5-methyl-1,2,4-oxadiazol-3-yl)phenoxy]propyl}-N-(11-hydroxyundecyl)isoxazole-3-carboxamide hemihydrate
by: K. Salorinne, et al.
Published: (2015-05-01)

Sonochemical synthesis of methyl-4-(hetero)arylmethylene isoxazole-5(4H)-ones using SnII-montmorillonite
by: Majid Ahmadzadeh, et al.
Published: (2018-04-01)

Modification, Characterization, and Catalytic Application of Mesolite for One Pot Synthesis of 3-Methyl-4-arylmethylene-isoxazol-5(4H)-ones
by: Ganesh Trambakrao Pawar, et al.
Published: (2017-04-01)

Crystal structure of ethyl 2-amino-4-(4-chlorophenyl)-4H-1-benzothieno[3,2-b]pyran-3-carboxylate
by: Mohamed Bakhouch, et al.
Published: (2015-08-01)

2-(4-Methoxybenzylidene)-4,4-dimethyl-3,4-dihydronaphthalen-1(2H)-one
by: Ghali Al Houari, et al.
Published: (2010-12-01)

3-(1-{[1-(4-Bromophenyl)-1H-1,2,3-triazol-4-yl]methyl}piperidin-4-yl)-6-fluoro-1,2-benzoxazole hemihydrate
by: N. Ashwini, et al.
Published: (2016-01-01)

9α-Hydroxy-4,8-dimethyl-3′-phenyl-3,14-dioxatricyclo[9.3.0.02,4]tetradec-7-en-13-one-12-spiro-5′-isoxazole monohydrate
by: Fatima Outahar, et al.
Published: (2019-10-01)

Synthesis and Antimicrobial Activity of N′-Heteroarylidene-1-adamantylcarbohydrazides and (±)-2-(1-Adamantyl)-4-acetyl-5-[5-(4-substituted phenyl-3-isoxazolyl)]-1,3,4-oxadiazolines
by: Abdul-Malek S. Al-Tamimi, et al.
Published: (2012-03-01)

Crystal structure of 1,5-diethyl-3′,5′-diphenyl-1,5-dihydro-3′H-spiro[pyrazolo[3,4-d]pyrimidine-4,2′-[1,3,4]thiadiazole]
by: Mohammed El Fal, et al.
Published: (2015-10-01)

(4S,5R)-3-(4-Chlorophenyl)-5-(4-methoxyphenyl)-4-methyl-1-phenyl-4,5-dihydro-1H-pyrazole
by: Yahya Ben Soumane, et al.
Published: (2016-06-01)

Synthesis and biological evaluation of (3-arylisoxazol-5-yl) methyl 6-fluoro-4-oxo-4H-chromene-2-carboxylates as antioxidant and antimicrobial agents
by: Battula Kumaraswamy, et al.
Published: (2017-01-01)

5-[(Benzo[d][1,3]dioxol-5-yl)methyl]-3-[4-(pyridin-2-yl)phenyl]-4,5-dihydroisoxazole
by: Nasseem El-Khatatneh, et al.
Published: (2017-02-01)

(2E)-4-tert-Butyl-2-(4-methoxybenzylidene)-3,4-dihydronaphthalen-1(2H)-one
by: Mohamed Akhazzane, et al.
Published: (2011-07-01)

Fluorescent Probes from Aromatic Polycyclic Nitrile Oxides: Isoxazoles versus Dihydro‐1λ3,3,2λ4‐Oxazaborinines
by: Dr. Mattia Moiola, et al.
Published: (2019-06-01)

Crystal structure of N-ethyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
by: Adriano Bof de Oliveira, et al.
Published: (2017-02-01)

Looking for a new antitubercular pharmacophore site: synthesis and bioactivity of spiroheterocycles 2,3',4'-tri-subsituted-1,2-dihydro-4H,4'H-spiro[isoquinoline-3,5'-isoxazol]-4-ones
by: Taibi Ben Hadda, et al.
Published: (2007-11-01)

Crystal structure of 3-benzylsulfanyl-6-(5-methyl-1,2-oxazol-3-yl)-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole
by: Krishnaiah Vaarla, et al.
Published: (2015-11-01)

Design and Synthesis of New 6-Nitro and 6-Amino-3,3a,4,5-Tetrahydro-2<i>H</i>-Benzo[<i>g</i>]indazole Derivatives: Antiproliferative and Antibacterial Activity
by: Viviana Cuartas, et al.
Published: (2019-11-01)

Crystal structure of ethyl 3-(4-chlorophenyl)-5-[(E)-2-(dimethylamino)ethenyl]-1,2-oxazole-4-carboxylate
by: Ilya Efimov, et al.
Published: (2015-12-01)

4-[(3-Phenyl-4,5-dihydroisoxazol-5-yl)methyl]-2H-benzo[b][1,4]thiazin-3(4H)-one
by: Nada Kheira Sebbar, et al.
Published: (2016-06-01)

Cannot write session to /tmp/vufind_sessions/sess_ch3ij8k7vge4a7ql46bpusft3o