Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites

Magnesium matrix composites synergistically reinforced by SiC nanoparticles and second phases were prepared by 12 passes of multi-pass forging, varying the temperature. The effects of grain refinement and the precipitates on the hot deformation behavior were analyzed. Deformation zones which could b...

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Main Authors: Kaibo Nie, Zhihao Zhu, Kunkun Deng, Ting Wang, Jungang Han
Format: Article
Language:English
Published: MDPI AG 2019-01-01
Series:Nanomaterials
Subjects:
Online Access:http://www.mdpi.com/2079-4991/9/1/57
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spelling doaj-84cec7f084624d2eb8d2cd9298d26c412020-11-25T00:13:44ZengMDPI AGNanomaterials2079-49912019-01-01915710.3390/nano9010057nano9010057Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix CompositesKaibo Nie0Zhihao Zhu1Kunkun Deng2Ting Wang3Jungang Han4College of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaCollege of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaCollege of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaCollege of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaCollege of Materials Science and Engineering, Taiyuan University of Technology, Taiyuan 030024, ChinaMagnesium matrix composites synergistically reinforced by SiC nanoparticles and second phases were prepared by 12 passes of multi-pass forging, varying the temperature. The effects of grain refinement and the precipitates on the hot deformation behavior were analyzed. Deformation zones which could be observed in the fine-grained nanocomposite before hot compression disappeared, and the trend of streamlined distribution for the precipitated phases was weakened. At the same compression rate, as the compression temperature increased, the number of precipitated phases decreased, and the grain size increased. For fine-grained nanocomposites, after the peak stress, there was no obvious dynamic softening stage on the stress–strain curve, and then the steady stage was quickly reached. The critical stress of the fine-grained nanocomposites was lower than that of the coarse-grained nanocomposites, which can be attributed to the large amounts of precipitates and significantly refined grains. The deformation mechanism of the coarse-grained nanocomposite was controlled by dislocation climb resulting from lattice diffusion, while the deformation mechanism for the fine-grained nanocomposite was dislocation climb resulting from grain boundary slip. The activation energy of the fine-grained nanocomposite was decreased, compared with the coarse-grained nanocomposite. The area of the workability region for the fine-grained nanocomposite was significantly larger than that of the coarse-grained nanocomposite, and there was no instability region at a low strain rate (0.001–0.01 s−1) under all deformation temperatures. The optimal workability region was 573 K /0.001–0.01 s−1 for the fine-grained nanocomposite, and the processing temperature was lower than the coarse-grained nanocomposite (623–673 K).http://www.mdpi.com/2079-4991/9/1/57magnesium matrix nanocompositeflow behaviordeformation mechanismprocessing map
collection DOAJ
language English
format Article
sources DOAJ
author Kaibo Nie
Zhihao Zhu
Kunkun Deng
Ting Wang
Jungang Han
spellingShingle Kaibo Nie
Zhihao Zhu
Kunkun Deng
Ting Wang
Jungang Han
Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
Nanomaterials
magnesium matrix nanocomposite
flow behavior
deformation mechanism
processing map
author_facet Kaibo Nie
Zhihao Zhu
Kunkun Deng
Ting Wang
Jungang Han
author_sort Kaibo Nie
title Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
title_short Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
title_full Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
title_fullStr Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
title_full_unstemmed Hot Deformation Behavior and Processing Maps of SiC Nanoparticles and Second Phase Synergistically Reinforced Magnesium Matrix Composites
title_sort hot deformation behavior and processing maps of sic nanoparticles and second phase synergistically reinforced magnesium matrix composites
publisher MDPI AG
series Nanomaterials
issn 2079-4991
publishDate 2019-01-01
description Magnesium matrix composites synergistically reinforced by SiC nanoparticles and second phases were prepared by 12 passes of multi-pass forging, varying the temperature. The effects of grain refinement and the precipitates on the hot deformation behavior were analyzed. Deformation zones which could be observed in the fine-grained nanocomposite before hot compression disappeared, and the trend of streamlined distribution for the precipitated phases was weakened. At the same compression rate, as the compression temperature increased, the number of precipitated phases decreased, and the grain size increased. For fine-grained nanocomposites, after the peak stress, there was no obvious dynamic softening stage on the stress–strain curve, and then the steady stage was quickly reached. The critical stress of the fine-grained nanocomposites was lower than that of the coarse-grained nanocomposites, which can be attributed to the large amounts of precipitates and significantly refined grains. The deformation mechanism of the coarse-grained nanocomposite was controlled by dislocation climb resulting from lattice diffusion, while the deformation mechanism for the fine-grained nanocomposite was dislocation climb resulting from grain boundary slip. The activation energy of the fine-grained nanocomposite was decreased, compared with the coarse-grained nanocomposite. The area of the workability region for the fine-grained nanocomposite was significantly larger than that of the coarse-grained nanocomposite, and there was no instability region at a low strain rate (0.001–0.01 s−1) under all deformation temperatures. The optimal workability region was 573 K /0.001–0.01 s−1 for the fine-grained nanocomposite, and the processing temperature was lower than the coarse-grained nanocomposite (623–673 K).
topic magnesium matrix nanocomposite
flow behavior
deformation mechanism
processing map
url http://www.mdpi.com/2079-4991/9/1/57
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