Synthesis of in situ reinforced silicon nitride composites

The objective of this work was to investigate the effect of two different sintering additives (CeO2 and Y2O3 + Al2O3), sintering time and amount of b-Si3N4 seeds on the densification, mechanical properties and microstructure of self-reinforced Si3N4 based composites obtained by pressureless sinterin...

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Bibliographic Details
Main Authors: LJILJANA ZIVKOVIC, ALEKSANDRA VUCKOVIC, SNEZANA BOSKOVIC
Format: Article
Language:English
Published: Serbian Chemical Society 2004-01-01
Series:Journal of the Serbian Chemical Society
Subjects:
Online Access:http://www.shd.org.yu/HtDocs/SHD/Vol69/No1/V69-No1-08.pdf
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Summary:The objective of this work was to investigate the effect of two different sintering additives (CeO2 and Y2O3 + Al2O3), sintering time and amount of b-Si3N4 seeds on the densification, mechanical properties and microstructure of self-reinforced Si3N4 based composites obtained by pressureless sintering. Preparation of b-Si3N4 seeds, also obtained by a pressureless sintering procedure, is described. Samples without seeds were prepared for comparison. The results imply that self-reinforced silicon nitride based composites with densities close to the theoretical values and with fracture toughness of 9.3 MPa m1/2 can be obtained using a presureless sintering procedure.
ISSN:0352-5139