(E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide

(E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide

The title compound, C16H21FN2O3S, was obtained from the reaction between sulfonyl azide, cyclohexanone and morpholine. The bond lengths at the amidine N—C—N grouping are similar [1.326 (3) and 1.338 (3) Å], indicating significant conjugation. The cyclopentyl moiety displays disorder of one of the me...

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Bibliographic Details
Main Authors: Ilya Efimov, Pavel Slepukhin, Nikolai Beliaev, Vasiliy Bakulev
Format: Article
Language:English
Published: International Union of Crystallography 2016-01-01
Series:IUCrData
Subjects:
crystal structure
amidines
transformation
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314616000134
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spelling doaj-82aad84ebe134c2a80930217696976a92020-11-24T23:24:47ZengInternational Union of CrystallographyIUCrData2414-31462016-01-0111x16001310.1107/S2414314616000134hb4006(E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamideIlya Efimov0Pavel Slepukhin1Nikolai Beliaev2Vasiliy Bakulev3Ural Federal University, Mira 19 Ekaterinburg 620002, Russian FederationI. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of Russian Academy, of Sciences, 20 S. Kovalevskaya str., 620990 Ekaterinburg, RussiaUral Federal University, Mira 19 Ekaterinburg 620002, Russian FederationUral Federal University, Mira 19 Ekaterinburg 620002, Russian FederationThe title compound, C16H21FN2O3S, was obtained from the reaction between sulfonyl azide, cyclohexanone and morpholine. The bond lengths at the amidine N—C—N grouping are similar [1.326 (3) and 1.338 (3) Å], indicating significant conjugation. The cyclopentyl moiety displays disorder of one of the methylene groups into two orientations with occupancy coefficients 0.75/0.25. No shortened intermolecular contacts in the crystal are observed.http://scripts.iucr.org/cgi-bin/paper?S2414314616000134crystal structureamidinestransformation
collection DOAJ
language English
format Article
sources DOAJ
author Ilya Efimov
Pavel Slepukhin
Nikolai Beliaev
Vasiliy Bakulev
spellingShingle Ilya Efimov
Pavel Slepukhin
Nikolai Beliaev
Vasiliy Bakulev
(E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
IUCrData
crystal structure
amidines
transformation
author_facet Ilya Efimov
Pavel Slepukhin
Nikolai Beliaev
Vasiliy Bakulev
author_sort Ilya Efimov
title (E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
title_short (E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
title_full (E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
title_fullStr (E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
title_full_unstemmed (E)-N-[Cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
title_sort (e)-n-[cyclopentyl(morpholin-4-yl)methylidene]-4-fluorobenzenesulfonamide
publisher International Union of Crystallography
series IUCrData
issn 2414-3146
publishDate 2016-01-01
description The title compound, C16H21FN2O3S, was obtained from the reaction between sulfonyl azide, cyclohexanone and morpholine. The bond lengths at the amidine N—C—N grouping are similar [1.326 (3) and 1.338 (3) Å], indicating significant conjugation. The cyclopentyl moiety displays disorder of one of the methylene groups into two orientations with occupancy coefficients 0.75/0.25. No shortened intermolecular contacts in the crystal are observed.
topic crystal structure
amidines
transformation
url http://scripts.iucr.org/cgi-bin/paper?S2414314616000134
work_keys_str_mv AT ilyaefimov encyclopentylmorpholin4ylmethylidene4fluorobenzenesulfonamide
AT pavelslepukhin encyclopentylmorpholin4ylmethylidene4fluorobenzenesulfonamide
AT nikolaibeliaev encyclopentylmorpholin4ylmethylidene4fluorobenzenesulfonamide
AT vasiliybakulev encyclopentylmorpholin4ylmethylidene4fluorobenzenesulfonamide
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