Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
Abstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs succes...
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2021-07-01
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Online Access: | https://doi.org/10.1038/s41598-021-93514-z |
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doaj-7c3284d8db4a4fad9a088311fc800a4d2021-07-25T11:24:45ZengNature Publishing GroupScientific Reports2045-23222021-07-0111111410.1038/s41598-021-93514-zAnalysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connectionYuri Shinohara0Satomu Akabane1Tomonari Inamura2Laboratory for Materials and Structures, Tokyo Institute of TechnologyTokyo Institute of TechnologyLaboratory for Materials and Structures, Tokyo Institute of TechnologyAbstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs successfully explained their observed frequency; in the actual microstructure, variant pairs with a small θ form preferentially. The experimentally obtained JPs were consistent with theoretical ones. To the best of our knowledge, this is the first study to confirm the validity of variant-pair crystallography in steel based on rank-1 connection, both theoretically and experimentally. Diamond, composite-spear, and composite-kink clusters are considered. The cumulative θ at the JPs can suppress diamond cluster formation because it exceeds the θ of a single variant pair, and the diamond cluster is not observed experimentally. However, θ at the JPs cancel out in composite-spear (CS) and composite-kink (CK) clusters, but CK clusters are rarely observed experimentally, while a few CS clusters are observed. This demonstrates the analytical limitations of 2D approaches used to evaluate the frequency of variant pairs and clusters. These two variant clusters have a narrow window of 2D observation because the orientation relationships between JPs and intersection lines between two habit planes affect the areas of JPs.https://doi.org/10.1038/s41598-021-93514-z |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Yuri Shinohara Satomu Akabane Tomonari Inamura |
spellingShingle |
Yuri Shinohara Satomu Akabane Tomonari Inamura Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection Scientific Reports |
author_facet |
Yuri Shinohara Satomu Akabane Tomonari Inamura |
author_sort |
Yuri Shinohara |
title |
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
title_short |
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
title_full |
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
title_fullStr |
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
title_full_unstemmed |
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
title_sort |
analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection |
publisher |
Nature Publishing Group |
series |
Scientific Reports |
issn |
2045-2322 |
publishDate |
2021-07-01 |
description |
Abstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs successfully explained their observed frequency; in the actual microstructure, variant pairs with a small θ form preferentially. The experimentally obtained JPs were consistent with theoretical ones. To the best of our knowledge, this is the first study to confirm the validity of variant-pair crystallography in steel based on rank-1 connection, both theoretically and experimentally. Diamond, composite-spear, and composite-kink clusters are considered. The cumulative θ at the JPs can suppress diamond cluster formation because it exceeds the θ of a single variant pair, and the diamond cluster is not observed experimentally. However, θ at the JPs cancel out in composite-spear (CS) and composite-kink (CK) clusters, but CK clusters are rarely observed experimentally, while a few CS clusters are observed. This demonstrates the analytical limitations of 2D approaches used to evaluate the frequency of variant pairs and clusters. These two variant clusters have a narrow window of 2D observation because the orientation relationships between JPs and intersection lines between two habit planes affect the areas of JPs. |
url |
https://doi.org/10.1038/s41598-021-93514-z |
work_keys_str_mv |
AT yurishinohara analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection AT satomuakabane analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection AT tomonariinamura analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection |
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1721283192342708224 |