Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection

Abstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs succes...

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Main Authors: Yuri Shinohara, Satomu Akabane, Tomonari Inamura
Format: Article
Language:English
Published: Nature Publishing Group 2021-07-01
Series:Scientific Reports
Online Access:https://doi.org/10.1038/s41598-021-93514-z
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spelling doaj-7c3284d8db4a4fad9a088311fc800a4d2021-07-25T11:24:45ZengNature Publishing GroupScientific Reports2045-23222021-07-0111111410.1038/s41598-021-93514-zAnalysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connectionYuri Shinohara0Satomu Akabane1Tomonari Inamura2Laboratory for Materials and Structures, Tokyo Institute of TechnologyTokyo Institute of TechnologyLaboratory for Materials and Structures, Tokyo Institute of TechnologyAbstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs successfully explained their observed frequency; in the actual microstructure, variant pairs with a small θ form preferentially. The experimentally obtained JPs were consistent with theoretical ones. To the best of our knowledge, this is the first study to confirm the validity of variant-pair crystallography in steel based on rank-1 connection, both theoretically and experimentally. Diamond, composite-spear, and composite-kink clusters are considered. The cumulative θ at the JPs can suppress diamond cluster formation because it exceeds the θ of a single variant pair, and the diamond cluster is not observed experimentally. However, θ at the JPs cancel out in composite-spear (CS) and composite-kink (CK) clusters, but CK clusters are rarely observed experimentally, while a few CS clusters are observed. This demonstrates the analytical limitations of 2D approaches used to evaluate the frequency of variant pairs and clusters. These two variant clusters have a narrow window of 2D observation because the orientation relationships between JPs and intersection lines between two habit planes affect the areas of JPs.https://doi.org/10.1038/s41598-021-93514-z
collection DOAJ
language English
format Article
sources DOAJ
author Yuri Shinohara
Satomu Akabane
Tomonari Inamura
spellingShingle Yuri Shinohara
Satomu Akabane
Tomonari Inamura
Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
Scientific Reports
author_facet Yuri Shinohara
Satomu Akabane
Tomonari Inamura
author_sort Yuri Shinohara
title Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
title_short Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
title_full Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
title_fullStr Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
title_full_unstemmed Analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
title_sort analysis of variant-pairing tendencies in lenticular martensite microstructures based on rank-1 connection
publisher Nature Publishing Group
series Scientific Reports
issn 2045-2322
publishDate 2021-07-01
description Abstract Herein, variant-pairing tendencies of lenticular martensite in an Fe–30Ni–0.3C (wt%) alloy are analyzed based on rank-1 connection at martensite/martensite junction planes (JPs) to facilitate the understanding of martensite microstructure. The degree of incompatibility (θ) at the JPs successfully explained their observed frequency; in the actual microstructure, variant pairs with a small θ form preferentially. The experimentally obtained JPs were consistent with theoretical ones. To the best of our knowledge, this is the first study to confirm the validity of variant-pair crystallography in steel based on rank-1 connection, both theoretically and experimentally. Diamond, composite-spear, and composite-kink clusters are considered. The cumulative θ at the JPs can suppress diamond cluster formation because it exceeds the θ of a single variant pair, and the diamond cluster is not observed experimentally. However, θ at the JPs cancel out in composite-spear (CS) and composite-kink (CK) clusters, but CK clusters are rarely observed experimentally, while a few CS clusters are observed. This demonstrates the analytical limitations of 2D approaches used to evaluate the frequency of variant pairs and clusters. These two variant clusters have a narrow window of 2D observation because the orientation relationships between JPs and intersection lines between two habit planes affect the areas of JPs.
url https://doi.org/10.1038/s41598-021-93514-z
work_keys_str_mv AT yurishinohara analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection
AT satomuakabane analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection
AT tomonariinamura analysisofvariantpairingtendenciesinlenticularmartensitemicrostructuresbasedonrank1connection
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