Microstructure and Flux Pinning of Reacted-and-Pressed, Polycrystalline Ba<sub>0.6</sub>K<sub>0.4</sub>Fe<sub>2</sub>As<sub>2</sub> Powders

The flux pinning properties of reacted-and-pressed Ba<sub>0.6</sub>K<sub>0.4</sub>Fe<sub>2</sub>As<sub>2</sub> powder were measured using magnetic hysteresis loops in the temperature range 20 K &#8804; <i>T</i> &#8804; 35 K. The sca...

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Bibliographic Details
Main Authors: Michael R. Koblischka, Anjela Koblischka-Veneva, Jörg Schmauch, Masato Murakami
Format: Article
Language:English
Published: MDPI AG 2019-07-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/12/13/2173
Description
Summary:The flux pinning properties of reacted-and-pressed Ba<sub>0.6</sub>K<sub>0.4</sub>Fe<sub>2</sub>As<sub>2</sub> powder were measured using magnetic hysteresis loops in the temperature range 20 K &#8804; <i>T</i> &#8804; 35 K. The scaling analysis of the flux pinning forces (<inline-formula> <math display="inline"> <semantics> <mrow> <msub> <mi>F</mi> <mi>p</mi> </msub> <mo>=</mo> <msub> <mi>j</mi> <mi>c</mi> </msub> <mo>&#215;</mo> <mi>B</mi> </mrow> </semantics> </math> </inline-formula>, with <inline-formula> <math display="inline"> <semantics> <msub> <mi>j</mi> <mi>c</mi> </msub> </semantics> </math> </inline-formula> denoting the critical current density) following the Dew-Hughes model reveals a dominant flux pinning provided by normal-conducting point defects (<inline-formula> <math display="inline"> <semantics> <mrow> <mi>&#948;</mi> <mi>l</mi> </mrow> </semantics> </math> </inline-formula>-pinning) with only small irreversibility fields, <inline-formula> <math display="inline"> <semantics> <msub> <mi>H</mi> <mi>irr</mi> </msub> </semantics> </math> </inline-formula>, ranging between 0.5 T (35 K) and 16 T (20 K). Kramer plots demonstrate a linear behavior above an applied field of 0.6 T. The samples were further characterized by electron backscatter diffraction (EBSD) analysis to elucidate the origin of the flux pinning. We compare our data with results of Weiss et al. (bulks) and Yao et al. (tapes), revealing that the dominant flux pinning in the samples for applications is provided mainly by grain boundary pinning, created by the densification procedures and the mechanical deformation applied.
ISSN:1996-1944