Summary: | Fe<sub>3</sub>O<sub>4</sub> decorated graphene was synthesized for electromagnetic wave absorption via a facile one-pot hydrothermal approach. The structure and morphology of the as-prepared nanomaterials were systematically investigated. The graphene oxide (GO) was reduced and Fe<sub>3</sub>O<sub>4</sub> nanoparticles were evenly decorated on the surface of reduced graphene oxide (rGO) nanosheets. The average particle size of Fe<sub>3</sub>O<sub>4</sub> nanoparticles is about 15.3 nm. The as-prepared rGO-Fe<sub>3</sub>O<sub>4</sub> nanocomposites exhibited a good microwave absorption performance because of the combination of graphene and magnetic Fe<sub>3</sub>O<sub>4</sub>. When the thicknesses are 1.6 mm and 6.5 mm, the reflection loss (RL) values are up to −34.4 dB and −37.5 dB, respectively. The effective bandwidths are 3.8 and 1.9 GHz.
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