Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)

Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)

The crystal structure of the title compound, [Sn(C5H10NS2)4], was originally determined by Harreld & Schlemper [Acta Cryst. (1971), B27, 1964–1969] using intensity data estimated from Weissenberg films. In comparison with the previous refinement, the current redetermination...

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Main Authors: Coco K. Y. A. Okio, Nivaldo L. Speziali
Format: Article
Language:English
Published: International Union of Crystallography 2009-06-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809018522
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spelling doaj-78edd06897d74dcd9810b60cd35883f72020-11-25T00:20:49ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-06-01656m675m67510.1107/S1600536809018522Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)Coco K. Y. A. OkioNivaldo L. SpezialiThe crystal structure of the title compound, [Sn(C5H10NS2)4], was originally determined by Harreld & Schlemper [Acta Cryst. (1971), B27, 1964–1969] using intensity data estimated from Weissenberg films. In comparison with the previous refinement, the current redetermination reveals anisotropic displacement parameters for all non-H atoms, localization of the H atoms, and higher precision of lattice parameters and interatomic distances. The complex features a distorted S6 octahedral coordination geometry for tin and a cis disposition of the monodentate dithiocarbamate ligands. http://scripts.iucr.org/cgi-bin/paper?S1600536809018522
collection DOAJ
language English
format Article
sources DOAJ
author Coco K. Y. A. Okio
Nivaldo L. Speziali
spellingShingle Coco K. Y. A. Okio
Nivaldo L. Speziali
Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
Acta Crystallographica Section E
author_facet Coco K. Y. A. Okio
Nivaldo L. Speziali
author_sort Coco K. Y. A. Okio
title Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
title_short Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
title_full Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
title_fullStr Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
title_full_unstemmed Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)
title_sort redetermination of tetrakis(n,n-diethyldithiocarbamato)tin(iv)
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-06-01
description The crystal structure of the title compound, [Sn(C5H10NS2)4], was originally determined by Harreld & Schlemper [Acta Cryst. (1971), B27, 1964–1969] using intensity data estimated from Weissenberg films. In comparison with the previous refinement, the current redetermination reveals anisotropic displacement parameters for all non-H atoms, localization of the H atoms, and higher precision of lattice parameters and interatomic distances. The complex features a distorted S6 octahedral coordination geometry for tin and a cis disposition of the monodentate dithiocarbamate ligands.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809018522
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AT nivaldolspeziali redeterminationoftetrakisnndiethyldithiocarbamatotiniv
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