7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate

7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate

In the racemic title compound, C34H22Br2N2S·CDCl3, pairs of diquinoline host molecules form centrosymmetric brick-like dimers utilizing three different aryl edge-to-face interactions (EF1–3). The dimeric (EF)6 (i.e. 2 × EF1–3) building blocks pac...

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Main Authors: Isa Y. H. Chan, Roger Bishop, Donald C. Craig, Mohan M. Bhadbhade, Marcia L. Scudder
Format: Article
Language:English
Published: International Union of Crystallography 2009-09-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809032978
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spelling doaj-74c10184906b4fb2a58b5f02c2fa6a842020-11-25T01:00:17ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-09-01659o2253o225310.1107/S16005368090329787α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvateIsa Y. H. ChanRoger BishopDonald C. CraigMohan M. BhadbhadeMarcia L. ScudderIn the racemic title compound, C34H22Br2N2S·CDCl3, pairs of diquinoline host molecules form centrosymmetric brick-like dimers utilizing three different aryl edge-to-face interactions (EF1–3). The dimeric (EF)6 (i.e. 2 × EF1–3) building blocks pack with the deuterochloroform guest molecules positioned near each of their corners. The Cl atoms of the latter are disordered over two sets of sites in a 0.53 (2):0.47 (2) ratio. http://scripts.iucr.org/cgi-bin/paper?S1600536809032978
collection DOAJ
language English
format Article
sources DOAJ
author Isa Y. H. Chan
Roger Bishop
Donald C. Craig
Mohan M. Bhadbhade
Marcia L. Scudder
spellingShingle Isa Y. H. Chan
Roger Bishop
Donald C. Craig
Mohan M. Bhadbhade
Marcia L. Scudder
7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
Acta Crystallographica Section E
author_facet Isa Y. H. Chan
Roger Bishop
Donald C. Craig
Mohan M. Bhadbhade
Marcia L. Scudder
author_sort Isa Y. H. Chan
title 7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
title_short 7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
title_full 7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
title_fullStr 7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
title_full_unstemmed 7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
title_sort 7α,15α-dibromo-8,16-diphenyl-6,7,14,15-tetrahydro-6α,14α-epithiocycloocta[1,2-b:5,6-b′]diquinoline deuterochloroform solvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-09-01
description In the racemic title compound, C34H22Br2N2S·CDCl3, pairs of diquinoline host molecules form centrosymmetric brick-like dimers utilizing three different aryl edge-to-face interactions (EF1–3). The dimeric (EF)6 (i.e. 2 × EF1–3) building blocks pack with the deuterochloroform guest molecules positioned near each of their corners. The Cl atoms of the latter are disordered over two sets of sites in a 0.53 (2):0.47 (2) ratio.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809032978
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AT rogerbishop 7amp94515amp945dibromo816diphenyl671415tetrahydro6amp94514amp945epithiocycloocta12b56bamp8242diquinolinedeuterochloroformsolvate
AT donaldccraig 7amp94515amp945dibromo816diphenyl671415tetrahydro6amp94514amp945epithiocycloocta12b56bamp8242diquinolinedeuterochloroformsolvate
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AT marcialscudder 7amp94515amp945dibromo816diphenyl671415tetrahydro6amp94514amp945epithiocycloocta12b56bamp8242diquinolinedeuterochloroformsolvate
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