Synthesis and 3D-AFM surface topology of nanographene-like material extracted from sulfonated tri-, di- and monochloroacetic acid
In this study a graphene-like material was synthesized by chemical exfoliation of sieved graphite powder with an average particles size ≤100 µm in dispersing medium from tri-, di- and monochloroacetic acid sulfonated with 55 % H2SO3. The results indicated that the yield of graphene-like material was...
| Main Author: | |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Sciendo
2016-09-01
|
| Series: | Materials Science-Poland |
| Subjects: | |
| Online Access: | https://doi.org/10.1515/msp-2016-0081 |
| Summary: | In this study a graphene-like material was synthesized by chemical exfoliation of sieved graphite powder with an average particles size ≤100 µm in dispersing medium from tri-, di- and monochloroacetic acid sulfonated with 55 % H2SO3. The results indicated that the yield of graphene-like material was the best in case of trichloroacetic 55 % H2SO3, taking into account structure quality and amount of obtained material. Layered graphene-like material was carefully collected after reduction of GO formed by 50 % dimethylhydrazine. AFM-investigations were performed to characterize nanostructural features of produced graphene and expected surface area which is surface topology dependent. Furthermore, Raman spectra were measured to confirm graphene formation. |
|---|---|
| ISSN: | 2083-134X |