Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone

Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone

Diarylidene acetones (DAA) (1-5) had been prepared by the condensation of acetone with substituted benzaldehydes via Claisen-Schmidt reaction, DAA’s brought to condense with anthrone to afford the title compounds (6-10) through Michael addition. The structures of the products were suggested in the l...

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Bibliographic Details
Main Authors: Mohammed S. Hussein, Abdul Wahab J. Al-Hamdany, Rana A. Saeed
Format: Article
Language:English
Published: University of Zakho 2018-12-01
Series:Science Journal of University of Zakho
Subjects:
Anthrone
spirocyclohexanones
Michael addition
Online Access:https://sjuoz.uoz.edu.krd/index.php/sjuoz/article/view/548
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spelling doaj-70626361b4504cdc9d1f56ec8e5ba26c2020-11-25T02:41:37Zeng University of ZakhoScience Journal of University of Zakho2663-628X2663-62982018-12-016415515910.25271/sjuoz.2018.6.4.548548Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from AcetoneMohammed S. Hussein0Abdul Wahab J. Al-Hamdany1Rana A. Saeed2Department of Chemistry, Faculty of Science, University of Zakho, Kurdistan Region - Iraq - (mohammed.huseein@uoz.edu.krd)Department of Chemistry, College of Science, University of Mosul, Mosul, Iraq - (ajalhamadany@yahoo.com)Department of Pharmacy, Technical InstituteNorthern Technical University, Mosul, Iraq - (rana.al_alaf@yahoo.com)Diarylidene acetones (DAA) (1-5) had been prepared by the condensation of acetone with substituted benzaldehydes via Claisen-Schmidt reaction, DAA’s brought to condense with anthrone to afford the title compounds (6-10) through Michael addition. The structures of the products were suggested in the light of spectral data (UV, IR, 1H&13C-NMR).https://sjuoz.uoz.edu.krd/index.php/sjuoz/article/view/548AnthronespirocyclohexanonesMichael addition
collection DOAJ
language English
format Article
sources DOAJ
author Mohammed S. Hussein
Abdul Wahab J. Al-Hamdany
Rana A. Saeed
spellingShingle Mohammed S. Hussein
Abdul Wahab J. Al-Hamdany
Rana A. Saeed
Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
Science Journal of University of Zakho
Anthrone
spirocyclohexanones
Michael addition
author_facet Mohammed S. Hussein
Abdul Wahab J. Al-Hamdany
Rana A. Saeed
author_sort Mohammed S. Hussein
title Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
title_short Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
title_full Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
title_fullStr Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
title_full_unstemmed Synthesis and Spectral Characterization of Some New Substituted Bis-spirocyclohexanones Derived from Acetone
title_sort synthesis and spectral characterization of some new substituted bis-spirocyclohexanones derived from acetone
publisher University of Zakho
series Science Journal of University of Zakho
issn 2663-628X
2663-6298
publishDate 2018-12-01
description Diarylidene acetones (DAA) (1-5) had been prepared by the condensation of acetone with substituted benzaldehydes via Claisen-Schmidt reaction, DAA’s brought to condense with anthrone to afford the title compounds (6-10) through Michael addition. The structures of the products were suggested in the light of spectral data (UV, IR, 1H&13C-NMR).
topic Anthrone
spirocyclohexanones
Michael addition
url https://sjuoz.uoz.edu.krd/index.php/sjuoz/article/view/548
work_keys_str_mv AT mohammedshussein synthesisandspectralcharacterizationofsomenewsubstitutedbisspirocyclohexanonesderivedfromacetone
AT abdulwahabjalhamdany synthesisandspectralcharacterizationofsomenewsubstitutedbisspirocyclohexanonesderivedfromacetone
AT ranaasaeed synthesisandspectralcharacterizationofsomenewsubstitutedbisspirocyclohexanonesderivedfromacetone
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