Synthesis of Biodiesel in Microstructured Reactors under Supercritical Reaction Conditions
At IMM the advantages of an alternative synthesis route for biodiesel under supercritical conditions in micro-structured reactors applying heterogeneous catalysts are currently under investigation. Target of the development work is to build a pilot plant with an annual production capacity of 40 t wh...
| Main Authors: | , , , , |
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| Format: | Article |
| Language: | English |
| Published: |
AIDIC Servizi S.r.l.
2014-06-01
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| Series: | Chemical Engineering Transactions |
| Online Access: | https://www.cetjournal.it/index.php/cet/article/view/5785 |
| Summary: | At IMM the advantages of an alternative synthesis route for biodiesel under supercritical conditions in micro-structured reactors applying heterogeneous catalysts are currently under investigation. Target of the development work is to build a pilot plant with an annual production capacity of 40 t which covers all process engineering steps and verifies their functionality in laboratory and field trials. The supercritical process applying catalysts has not been investigated in a continuous plant to date.
The development work covers so far the optimization of the supercritical process conditions in absence of catalyst, which revealed full conversion in less than 5 min residence time. The preliminary screening of heterogeneous catalysts applying a model feed (Tricaprin) revealed full conversion in less than 30 s residence time over alumina catalysts. Based upon an ASPEN model of the process, a flow scheme of the future plant was set up. |
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| ISSN: | 2283-9216 |