Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films

A multi-aperture shower design is reported to improve the transverse uniformity of GdYBCO superconducting films on the template of sputtered-LaMnO3/epitaxial-MgO/IBAD-MgO/solution deposition planarization (SDP)-Y2O3-buffered Hastelloy tapes. The GdYBCO films were prepared by the metal organic chemic...

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Main Authors: Ruipeng Zhao, Qing Liu, Yudong Xia, Fei Zhang, Yuming Lu, Chuanbing Cai, Bowan Tao, Yanrong Li
Format: Article
Language:English
Published: MDPI AG 2017-09-01
Series:Materials
Subjects:
Online Access:https://www.mdpi.com/1996-1944/10/9/1088
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spelling doaj-6fcd9f71be974a75be3a0b6b5eb451022020-11-24T22:37:35ZengMDPI AGMaterials1996-19442017-09-01109108810.3390/ma10091088ma10091088Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO FilmsRuipeng Zhao0Qing Liu1Yudong Xia2Fei Zhang3Yuming Lu4Chuanbing Cai5Bowan Tao6Yanrong Li7State Key Lab of Electronic Thin Films and Integrated Devices, University of Electronic Science and Technology of China, Chengdu 610054, ChinaState Key Lab of Electronic Thin Films and Integrated Devices, University of Electronic Science and Technology of China, Chengdu 610054, ChinaSchool of Physical Science and Technology, Southwest Jiaotong University, Chengdu 610031, ChinaChengdu Fine Optical Engineering Research Center, Chengdu 610041, ChinaSchool of Physics, Shanghai University, Shanghai 200444, ChinaSchool of Physics, Shanghai University, Shanghai 200444, ChinaState Key Lab of Electronic Thin Films and Integrated Devices, University of Electronic Science and Technology of China, Chengdu 610054, ChinaState Key Lab of Electronic Thin Films and Integrated Devices, University of Electronic Science and Technology of China, Chengdu 610054, ChinaA multi-aperture shower design is reported to improve the transverse uniformity of GdYBCO superconducting films on the template of sputtered-LaMnO3/epitaxial-MgO/IBAD-MgO/solution deposition planarization (SDP)-Y2O3-buffered Hastelloy tapes. The GdYBCO films were prepared by the metal organic chemical vapor deposition (MOCVD) process. The transverse uniformities of structure, morphology, thickness, and performance were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), step profiler, and the standard four-probe method using the criteria of 1 μV/cm, respectively. Through adopting the multi-aperture shower instead of the slit shower, measurement by step profiler revealed that the thickness difference between the middle and the edges based on the slit shower design was well eliminated. Characterization by SEM showed that a GdYBCO film with a smooth surface was successfully prepared. Moreover, the transport critical current density (Jc) of its middle and edge positions at 77 K and self-field were found to be over 5 MA/cm2 through adopting the micro-bridge four-probe method.https://www.mdpi.com/1996-1944/10/9/1088multi-aperture showerGdYBCOMOCVDmorphologycritical current
collection DOAJ
language English
format Article
sources DOAJ
author Ruipeng Zhao
Qing Liu
Yudong Xia
Fei Zhang
Yuming Lu
Chuanbing Cai
Bowan Tao
Yanrong Li
spellingShingle Ruipeng Zhao
Qing Liu
Yudong Xia
Fei Zhang
Yuming Lu
Chuanbing Cai
Bowan Tao
Yanrong Li
Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
Materials
multi-aperture shower
GdYBCO
MOCVD
morphology
critical current
author_facet Ruipeng Zhao
Qing Liu
Yudong Xia
Fei Zhang
Yuming Lu
Chuanbing Cai
Bowan Tao
Yanrong Li
author_sort Ruipeng Zhao
title Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
title_short Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
title_full Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
title_fullStr Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
title_full_unstemmed Multi-Aperture Shower Design for the Improvement of the Transverse Uniformity of MOCVD-Derived GdYBCO Films
title_sort multi-aperture shower design for the improvement of the transverse uniformity of mocvd-derived gdybco films
publisher MDPI AG
series Materials
issn 1996-1944
publishDate 2017-09-01
description A multi-aperture shower design is reported to improve the transverse uniformity of GdYBCO superconducting films on the template of sputtered-LaMnO3/epitaxial-MgO/IBAD-MgO/solution deposition planarization (SDP)-Y2O3-buffered Hastelloy tapes. The GdYBCO films were prepared by the metal organic chemical vapor deposition (MOCVD) process. The transverse uniformities of structure, morphology, thickness, and performance were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), step profiler, and the standard four-probe method using the criteria of 1 μV/cm, respectively. Through adopting the multi-aperture shower instead of the slit shower, measurement by step profiler revealed that the thickness difference between the middle and the edges based on the slit shower design was well eliminated. Characterization by SEM showed that a GdYBCO film with a smooth surface was successfully prepared. Moreover, the transport critical current density (Jc) of its middle and edge positions at 77 K and self-field were found to be over 5 MA/cm2 through adopting the micro-bridge four-probe method.
topic multi-aperture shower
GdYBCO
MOCVD
morphology
critical current
url https://www.mdpi.com/1996-1944/10/9/1088
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