5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate

We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1H-Nuclear Magnetic Resonance...

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Main Authors:	Maya Damayanti Rahayu, Susi Kusumaningrum, Hayun Hayun
Format:	Article
Language:	English
Published:	MDPI AG 2018-12-01
Series:	Molbank
Subjects:	1-O-acetyl-xanthorrhizol xanthorrizol oxidation potassium permanganate
Online Access:	http://www.mdpi.com/1422-8599/2019/1/M1041

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record_format	Article
spelling	doaj-6dbd4cb0f840492aad7801bdceaa08142020-11-24T22:05:38ZengMDPI AGMolbank1422-85992018-12-0120191M104110.3390/M1041M10415-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl AcetateMaya Damayanti Rahayu0Susi Kusumaningrum1Hayun Hayun2Center of Technology For Pharmaceutical and Medical, Agency for the Assessment and Application of Technology (BPPT), Jl. M.H Thamrin 8, Jakarta 10340, IndonesiaCenter of Technology For Pharmaceutical and Medical, Agency for the Assessment and Application of Technology (BPPT), Jl. M.H Thamrin 8, Jakarta 10340, IndonesiaFaculty of Pharmacy, Universitas Indonesia, Depok 1424, IndonesiaWe synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1H-Nuclear Magnetic Resonance (NMR) and 13C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.http://www.mdpi.com/1422-8599/2019/1/M10411-O-acetyl-xanthorrhizolxanthorrizoloxidationpotassium permanganate
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Maya Damayanti Rahayu Susi Kusumaningrum Hayun Hayun
spellingShingle	Maya Damayanti Rahayu Susi Kusumaningrum Hayun Hayun 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate Molbank 1-O-acetyl-xanthorrhizol xanthorrizol oxidation potassium permanganate
author_facet	Maya Damayanti Rahayu Susi Kusumaningrum Hayun Hayun
author_sort	Maya Damayanti Rahayu
title	5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate
title_short	5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate
title_full	5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate
title_fullStr	5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate
title_full_unstemmed	5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate
title_sort	5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate
publisher	MDPI AG
series	Molbank
issn	1422-8599
publishDate	2018-12-01
description	We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1H-Nuclear Magnetic Resonance (NMR) and 13C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.
topic	1-O-acetyl-xanthorrhizol xanthorrizol oxidation potassium permanganate
url	http://www.mdpi.com/1422-8599/2019/1/M1041
work_keys_str_mv	AT mayadamayantirahayu 56hydroxy6methyl5oxoheptan2yl2methylphenylacetate AT susikusumaningrum 56hydroxy6methyl5oxoheptan2yl2methylphenylacetate AT hayunhayun 56hydroxy6methyl5oxoheptan2yl2methylphenylacetate
_version_	1725825393692246016

5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl Phenyl Acetate

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