N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide

N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide

The asymmetric unit of the title compound, C22H18N4O2S2, contains two molecules. In one of them, the dihedral angles between the central benzene ring and the phenyl rings are 16.97 (8) and 20.97 (8)°, while the phenyl rings make a dihedral angle of 37.87 (8)&am...

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Main Authors: Zainab Ngaini, Maya Asyikin Mohd Ariff, Wan Sharifatun Handayani Wan Zullkiplee, Hasnain Hussain, Mohd Mustaqim Rosli
Format: Article
Language:English
Published: International Union of Crystallography 2013-09-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536813020163
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spelling doaj-6d6a94efdc3743a68fab15ea3543ca202020-11-25T02:09:18ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682013-09-01699o1374o137510.1107/S1600536813020163N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamideZainab NgainiMaya Asyikin Mohd AriffWan Sharifatun Handayani Wan ZullkipleeHasnain HussainMohd Mustaqim RosliThe asymmetric unit of the title compound, C22H18N4O2S2, contains two molecules. In one of them, the dihedral angles between the central benzene ring and the phenyl rings are 16.97 (8) and 20.97 (8)°, while the phenyl rings make a dihedral angle of 37.87 (8)°. In the other molecule, the corresponding values are 34.92 (7), 53.90 (7) and 60.68 (8)°, respectively. In each molecule, two intramolecular N—H...O hydrogen bonds generate S(6) rings and a short C—H...S contact also occurs. In the crystal, N—H...S, N—H...O, C—H...O and C—H...S interactions link the molecules into a three-dimensional network.http://scripts.iucr.org/cgi-bin/paper?S1600536813020163
collection DOAJ
language English
format Article
sources DOAJ
author Zainab Ngaini
Maya Asyikin Mohd Ariff
Wan Sharifatun Handayani Wan Zullkiplee
Hasnain Hussain
Mohd Mustaqim Rosli
spellingShingle Zainab Ngaini
Maya Asyikin Mohd Ariff
Wan Sharifatun Handayani Wan Zullkiplee
Hasnain Hussain
Mohd Mustaqim Rosli
N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
Acta Crystallographica Section E
author_facet Zainab Ngaini
Maya Asyikin Mohd Ariff
Wan Sharifatun Handayani Wan Zullkiplee
Hasnain Hussain
Mohd Mustaqim Rosli
author_sort Zainab Ngaini
title N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
title_short N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
title_full N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
title_fullStr N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
title_full_unstemmed N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
title_sort n,n′-bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2013-09-01
description The asymmetric unit of the title compound, C22H18N4O2S2, contains two molecules. In one of them, the dihedral angles between the central benzene ring and the phenyl rings are 16.97 (8) and 20.97 (8)°, while the phenyl rings make a dihedral angle of 37.87 (8)°. In the other molecule, the corresponding values are 34.92 (7), 53.90 (7) and 60.68 (8)°, respectively. In each molecule, two intramolecular N—H...O hydrogen bonds generate S(6) rings and a short C—H...S contact also occurs. In the crystal, N—H...S, N—H...O, C—H...O and C—H...S interactions link the molecules into a three-dimensional network.
url http://scripts.iucr.org/cgi-bin/paper?S1600536813020163
work_keys_str_mv AT zainabngaini nn8242bisphenylcarbamothioylbenzene13dicarboxamide
AT mayaasyikinmohdariff nn8242bisphenylcarbamothioylbenzene13dicarboxamide
AT wansharifatunhandayaniwanzullkiplee nn8242bisphenylcarbamothioylbenzene13dicarboxamide
AT hasnainhussain nn8242bisphenylcarbamothioylbenzene13dicarboxamide
AT mohdmustaqimrosli nn8242bisphenylcarbamothioylbenzene13dicarboxamide
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