Synthesis of Molecularly Imprinted Polymer for Sterol Separation

Synthesis of Molecularly Imprinted Polymer for Sterol Separation

Molecular imprinted polymer (MIP) was prepared by bulk polymerization in acetone using acrylamide as a functional monomer, ethylene glycol dimethacrylate as a crosslinker, stigmasterol as a template and benzoyl peroxide as an initiator. The obtained MIPs were characterized using a scanning electron...

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Main Authors: Yuangsawad Ratanaporn, Chuayrueng Nuengruthai, Nonthanasin Nattawat, Binabdullah Krittin, Na-Ranong Duangkamol
Format: Article
Language:English
Published: EDP Sciences 2016-01-01
Series:MATEC Web of Conferences
Online Access:http://dx.doi.org/10.1051/matecconf/20166204006
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spelling doaj-6d488b68f86b43b08547b416f0ef6cdb2021-02-02T00:15:53ZengEDP SciencesMATEC Web of Conferences2261-236X2016-01-01620400610.1051/matecconf/20166204006matecconf_iccfe2016_04006Synthesis of Molecularly Imprinted Polymer for Sterol SeparationYuangsawad Ratanaporn0Chuayrueng Nuengruthai1Nonthanasin Nattawat2Binabdullah Krittin3Na-Ranong Duangkamol4Division of Chemical Engineering, Faculty of Engineering, Rajamangala University of Technology KrungthepDepartment of Chemical Engineering, Faculty of Engineering, King Mongkut’s Institute of Technology LadkrabangDepartment of Chemical Engineering, Faculty of Engineering, King Mongkut’s Institute of Technology LadkrabangDepartment of Chemical Engineering, Faculty of Engineering, King Mongkut’s Institute of Technology LadkrabangDepartment of Chemical Engineering, Faculty of Engineering, King Mongkut’s Institute of Technology LadkrabangMolecular imprinted polymer (MIP) was prepared by bulk polymerization in acetone using acrylamide as a functional monomer, ethylene glycol dimethacrylate as a crosslinker, stigmasterol as a template and benzoyl peroxide as an initiator. The obtained MIPs were characterized using a scanning electron microscope and a fourier transform infrared spectrophotometer. Performance in sterol adsorption of MIPs prepared under various conditions was investigated using a model solution of phytosterols in heptane, comparing with a nonimprinted polymer (NIP). Statistical analysis revealed that the amounts of crosslinker and template strongly affected the performance of MIP while the amount of solvent slightly affected the performance of MIP. MIP synthesized under the optimal condition had adsorption capacity of 1.28 mgsterols/gads which were 1.13 times of NIP.http://dx.doi.org/10.1051/matecconf/20166204006
collection DOAJ
language English
format Article
sources DOAJ
author Yuangsawad Ratanaporn
Chuayrueng Nuengruthai
Nonthanasin Nattawat
Binabdullah Krittin
Na-Ranong Duangkamol
spellingShingle Yuangsawad Ratanaporn
Chuayrueng Nuengruthai
Nonthanasin Nattawat
Binabdullah Krittin
Na-Ranong Duangkamol
Synthesis of Molecularly Imprinted Polymer for Sterol Separation
MATEC Web of Conferences
author_facet Yuangsawad Ratanaporn
Chuayrueng Nuengruthai
Nonthanasin Nattawat
Binabdullah Krittin
Na-Ranong Duangkamol
author_sort Yuangsawad Ratanaporn
title Synthesis of Molecularly Imprinted Polymer for Sterol Separation
title_short Synthesis of Molecularly Imprinted Polymer for Sterol Separation
title_full Synthesis of Molecularly Imprinted Polymer for Sterol Separation
title_fullStr Synthesis of Molecularly Imprinted Polymer for Sterol Separation
title_full_unstemmed Synthesis of Molecularly Imprinted Polymer for Sterol Separation
title_sort synthesis of molecularly imprinted polymer for sterol separation
publisher EDP Sciences
series MATEC Web of Conferences
issn 2261-236X
publishDate 2016-01-01
description Molecular imprinted polymer (MIP) was prepared by bulk polymerization in acetone using acrylamide as a functional monomer, ethylene glycol dimethacrylate as a crosslinker, stigmasterol as a template and benzoyl peroxide as an initiator. The obtained MIPs were characterized using a scanning electron microscope and a fourier transform infrared spectrophotometer. Performance in sterol adsorption of MIPs prepared under various conditions was investigated using a model solution of phytosterols in heptane, comparing with a nonimprinted polymer (NIP). Statistical analysis revealed that the amounts of crosslinker and template strongly affected the performance of MIP while the amount of solvent slightly affected the performance of MIP. MIP synthesized under the optimal condition had adsorption capacity of 1.28 mgsterols/gads which were 1.13 times of NIP.
url http://dx.doi.org/10.1051/matecconf/20166204006
work_keys_str_mv AT yuangsawadratanaporn synthesisofmolecularlyimprintedpolymerforsterolseparation
AT chuayruengnuengruthai synthesisofmolecularlyimprintedpolymerforsterolseparation
AT nonthanasinnattawat synthesisofmolecularlyimprintedpolymerforsterolseparation
AT binabdullahkrittin synthesisofmolecularlyimprintedpolymerforsterolseparation
AT naranongduangkamol synthesisofmolecularlyimprintedpolymerforsterolseparation
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