Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating

The present paper reports the synthesis and characterization of mixed halide based formamidinium lead Perovskite nanoparticles having general formula [HC(NH2)2]PbInBr3-n. A single step low temperature chemical route using microwave reactor is reported. The Perovskites synthesized were characterized...

Full description

Bibliographic Details
Main Authors:	Rajib Saha, Samrat Paul
Format:	Article
Language:	English
Published:	Applied Science Innovations Private Limited 2019-06-01
Series:	Carbon: Science and Technology
Subjects:	Formamidinium Low temperature synthesis Mixed halide Microwave reactor Perovskite
Online Access:	http://www.applied-science-innovations.com/cst-web-site/CST-11-2-2019/CST-366-11-2-2019-124-129.pdf

id	doaj-6cec7c32284944fab3a1b42088031234
record_format	Article
spelling	doaj-6cec7c32284944fab3a1b420880312342020-11-25T02:04:12ZengApplied Science Innovations Private LimitedCarbon: Science and Technology0974-05460974-05462019-06-01112124129Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heatingRajib Saha0Samrat Paul1Advanced Materials Research and Energy Application Laboratory (AMREAL), Department of Energy Engineering, North-Eastern Hill University, Shillong - 793022, India.Advanced Materials Research and Energy Application Laboratory (AMREAL), Department of Energy Engineering, North-Eastern Hill University, Shillong - 793022, India.The present paper reports the synthesis and characterization of mixed halide based formamidinium lead Perovskite nanoparticles having general formula [HC(NH2)2]PbInBr3-n. A single step low temperature chemical route using microwave reactor is reported. The Perovskites synthesized were characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and Transmission electron microscopy (TEM). The X-ray diffraction revealed phase purity and tetragonal structure whereas TEM micrographs found that the synthesized particles are at 10-12 nm, 12-15 nm, 15- 20 nm and 20-22 nm for FAPbI3, FAPbBr3, FAPbBrI2 and FAPbIBr2 respectively. Optical properties and molecular bonding of the Perovskites was investigated by Fourier transform infra-red spectroscopy.http://www.applied-science-innovations.com/cst-web-site/CST-11-2-2019/CST-366-11-2-2019-124-129.pdfFormamidiniumLow temperature synthesisMixed halideMicrowave reactorPerovskite
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Rajib Saha Samrat Paul
spellingShingle	Rajib Saha Samrat Paul Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating Carbon: Science and Technology Formamidinium Low temperature synthesis Mixed halide Microwave reactor Perovskite
author_facet	Rajib Saha Samrat Paul
author_sort	Rajib Saha
title	Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating
title_short	Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating
title_full	Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating
title_fullStr	Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating
title_full_unstemmed	Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating
title_sort	synthesis of nh2ch5=nh2 based mixed halide perovskite nanoparticles using single step low temperature microwave assisted heating
publisher	Applied Science Innovations Private Limited
series	Carbon: Science and Technology
issn	0974-0546 0974-0546
publishDate	2019-06-01
description	The present paper reports the synthesis and characterization of mixed halide based formamidinium lead Perovskite nanoparticles having general formula [HC(NH2)2]PbInBr3-n. A single step low temperature chemical route using microwave reactor is reported. The Perovskites synthesized were characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR) and Transmission electron microscopy (TEM). The X-ray diffraction revealed phase purity and tetragonal structure whereas TEM micrographs found that the synthesized particles are at 10-12 nm, 12-15 nm, 15- 20 nm and 20-22 nm for FAPbI3, FAPbBr3, FAPbBrI2 and FAPbIBr2 respectively. Optical properties and molecular bonding of the Perovskites was investigated by Fourier transform infra-red spectroscopy.
topic	Formamidinium Low temperature synthesis Mixed halide Microwave reactor Perovskite
url	http://www.applied-science-innovations.com/cst-web-site/CST-11-2-2019/CST-366-11-2-2019-124-129.pdf
work_keys_str_mv	AT rajibsaha synthesisofnh2ch5nh2basedmixedhalideperovskitenanoparticlesusingsinglesteplowtemperaturemicrowaveassistedheating AT samratpaul synthesisofnh2ch5nh2basedmixedhalideperovskitenanoparticlesusingsinglesteplowtemperaturemicrowaveassistedheating
_version_	1724943875891527680

Synthesis of NH2CH5=NH2 based mixed halide Perovskite nanoparticles using single step low temperature microwave assisted heating

Similar Items