The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke

The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke

A gas chromatographic method for the determination of carbon monoxide and carbon dioxide in cigarette smoke was developed. A column containing Porapak Q packing and a cryogenic temperature programmer which employed liquid nitrogen to cool the column to subambient temperatures was used. The separatio...

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Main Authors: Morie G.P., Sloan C.H.
Format: Article
Language:English
Published: Sciendo 1972-08-01
Series:Beiträge zur Tabakforschung International
Online Access:https://doi.org/10.2478/cttr-2013-0289
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spelling doaj-6bd7758b3c0d4b65a17ba54b21b092dc2021-09-06T19:22:10ZengSciendoBeiträge zur Tabakforschung International1612-92371972-08-016417818110.2478/cttr-2013-0289The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette SmokeMorie G.P.0Sloan C.H.1Research Laboratories, Tennessee Eastman Company, Division of Eastman Kodak Company, Kingsport, Tennessee, USAResearch Laboratories, Tennessee Eastman Company, Division of Eastman Kodak Company, Kingsport, Tennessee, USAA gas chromatographic method for the determination of carbon monoxide and carbon dioxide in cigarette smoke was developed. A column containing Porapak Q packing and a cryogenic temperature programmer which employed liquid nitrogen to cool the column to subambient temperatures was used. The separation of N2, O2, CO, and CO2 was accomplished at temperatures of -70°C to 40°C, and the organic vapour phase of smoke was analysed as the column temperature was programmed to 220°C. The inorganic gases were detected by thermal conductivity and the organic vapours by flame ionization. The method was used to determine the amounts of carbon monoxide and carbon dioxide in the smoke of nonfilter, filter, and vented-filter cigarettes, and to analyse the organic vapour phase of smokehttps://doi.org/10.2478/cttr-2013-0289
collection DOAJ
language English
format Article
sources DOAJ
author Morie G.P.
Sloan C.H.
spellingShingle Morie G.P.
Sloan C.H.
The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
Beiträge zur Tabakforschung International
author_facet Morie G.P.
Sloan C.H.
author_sort Morie G.P.
title The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
title_short The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
title_full The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
title_fullStr The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
title_full_unstemmed The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke
title_sort use of cryogenic temperature gas chromatography for the determination of carbon monoxide and carbon dioxide in cigarette smoke
publisher Sciendo
series Beiträge zur Tabakforschung International
issn 1612-9237
publishDate 1972-08-01
description A gas chromatographic method for the determination of carbon monoxide and carbon dioxide in cigarette smoke was developed. A column containing Porapak Q packing and a cryogenic temperature programmer which employed liquid nitrogen to cool the column to subambient temperatures was used. The separation of N2, O2, CO, and CO2 was accomplished at temperatures of -70°C to 40°C, and the organic vapour phase of smoke was analysed as the column temperature was programmed to 220°C. The inorganic gases were detected by thermal conductivity and the organic vapours by flame ionization. The method was used to determine the amounts of carbon monoxide and carbon dioxide in the smoke of nonfilter, filter, and vented-filter cigarettes, and to analyse the organic vapour phase of smoke
url https://doi.org/10.2478/cttr-2013-0289
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