Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield

This study optimized a co-solvent free electrochemical method for biodiesel synthesis using graphite electrode and waste concrete heterogeneous catalyst. Various parameters were evaluated, including: applied voltage (9.6, 14.4, 19.2 V), catalyst particle size uniformity (unfiltered and filtered with...

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Main Authors: Wiyogo Prio Wicaksono, Sekar Asmara Jati, Ika Yanti, Prastika Krisma Jiwanti
Format: Article
Language:English
Published: Diponegoro University 2021-03-01
Series:Bulletin of Chemical Reaction Engineering & Catalysis
Subjects:
Online Access:https://ejournal2.undip.ac.id/index.php/bcrec/article/view/10310
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spelling doaj-69f78a191cda4f1eba5a2406a39e75722021-05-01T23:41:02ZengDiponegoro UniversityBulletin of Chemical Reaction Engineering & Catalysis1978-29932021-03-0116117918710.9767/bcrec.16.1.10310.179-1874705Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel YieldWiyogo Prio Wicaksono0Sekar Asmara Jati1Ika Yanti2Prastika Krisma Jiwanti3Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia , Jl. Kaliurang KM 14.5, Sleman, Yogyakarta, 55584, Indonesia; Research Center for Materials and Electrochemistry, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia, IndonesiaDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia , Jl. Kaliurang KM 14.5, Sleman, Yogyakarta, 55584, Indonesia; Research Center for Materials and Electrochemistry, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia, IndonesiaDepartment of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Islam Indonesia , Jl. Kaliurang KM 14.5, Sleman, Yogyakarta, 55584, IndonesiaNanotechnology Engineering, Faculty of Advanced Technology and Multidiscipline, Universitas Airlangga , Kampus C Universitas Airlangga, Surabaya, 60115, IndonesiaThis study optimized a co-solvent free electrochemical method for biodiesel synthesis using graphite electrode and waste concrete heterogeneous catalyst. Various parameters were evaluated, including: applied voltage (9.6, 14.4, 19.2 V), catalyst particle size uniformity (unfiltered and filtered with 150 mesh), and reaction time (15, 30, 120, 240 min). The results obtained 100% FAME content and 78.51% of biodiesel yield that were achieved at 14.4 V within 30 min using filtered catalyst and cooking oil feedstock. However, a slight decline was observed with the use of waste cooking oil. This optimized method offers a reliable and simple condition for mass biodiesel production. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).https://ejournal2.undip.ac.id/index.php/bcrec/article/view/10310electrochemical synthesisbiodieselwaste concreteheterogeneous catalystwaste cooking oil
collection DOAJ
language English
format Article
sources DOAJ
author Wiyogo Prio Wicaksono
Sekar Asmara Jati
Ika Yanti
Prastika Krisma Jiwanti
spellingShingle Wiyogo Prio Wicaksono
Sekar Asmara Jati
Ika Yanti
Prastika Krisma Jiwanti
Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
Bulletin of Chemical Reaction Engineering & Catalysis
electrochemical synthesis
biodiesel
waste concrete
heterogeneous catalyst
waste cooking oil
author_facet Wiyogo Prio Wicaksono
Sekar Asmara Jati
Ika Yanti
Prastika Krisma Jiwanti
author_sort Wiyogo Prio Wicaksono
title Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
title_short Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
title_full Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
title_fullStr Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
title_full_unstemmed Co-Solvent Free Electrochemical Synthesis of Biodiesel Using Graphite Electrode and Waste Concrete Heterogeneous Catalyst: Optimization of Biodiesel Yield
title_sort co-solvent free electrochemical synthesis of biodiesel using graphite electrode and waste concrete heterogeneous catalyst: optimization of biodiesel yield
publisher Diponegoro University
series Bulletin of Chemical Reaction Engineering & Catalysis
issn 1978-2993
publishDate 2021-03-01
description This study optimized a co-solvent free electrochemical method for biodiesel synthesis using graphite electrode and waste concrete heterogeneous catalyst. Various parameters were evaluated, including: applied voltage (9.6, 14.4, 19.2 V), catalyst particle size uniformity (unfiltered and filtered with 150 mesh), and reaction time (15, 30, 120, 240 min). The results obtained 100% FAME content and 78.51% of biodiesel yield that were achieved at 14.4 V within 30 min using filtered catalyst and cooking oil feedstock. However, a slight decline was observed with the use of waste cooking oil. This optimized method offers a reliable and simple condition for mass biodiesel production. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
topic electrochemical synthesis
biodiesel
waste concrete
heterogeneous catalyst
waste cooking oil
url https://ejournal2.undip.ac.id/index.php/bcrec/article/view/10310
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