Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate)
In the title compound, C29H25FN2O4, the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring sy...
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International Union of Crystallography
2017-11-01
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| Series: | Acta Crystallographica Section E: Crystallographic Communications |
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| Online Access: | http://scripts.iucr.org/cgi-bin/paper?S2056989017015523 |
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doaj-66a6a84e322a448e98c30fb5c4d2f78e2020-11-25T01:23:03ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902017-11-0173111790179210.1107/S2056989017015523xu5908Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate)Xin-Hua Lu0Hong-Shun Sun1Yuan Cai2Lu-Lu Chen3Yang-Feng Chen4Targeted MRI Contrast Agents Laboratory of Jiangsu Province, Nanjing Polytechnic Institute, Geguan Road No.265 Nanjing, Nanjing 210048, People's Republic of ChinaTargeted MRI Contrast Agents Laboratory of Jiangsu Province, Nanjing Polytechnic Institute, Geguan Road No.265 Nanjing, Nanjing 210048, People's Republic of ChinaTargeted MRI Contrast Agents Laboratory of Jiangsu Province, Nanjing Polytechnic Institute, Geguan Road No.265 Nanjing, Nanjing 210048, People's Republic of ChinaTargeted MRI Contrast Agents Laboratory of Jiangsu Province, Nanjing Polytechnic Institute, Geguan Road No.265 Nanjing, Nanjing 210048, People's Republic of ChinaTargeted MRI Contrast Agents Laboratory of Jiangsu Province, Nanjing Polytechnic Institute, Geguan Road No.265 Nanjing, Nanjing 210048, People's Republic of ChinaIn the title compound, C29H25FN2O4, the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring systems by 83.3 (2) and 88.1 (4)°, respectively. In the crystal, pairs of N—H...O hydrogen bonds link the molecules into centrosymmetric dimers, which are further linked by N—H...O hydrogen bonds into supramolecular chains propagating along the [101] direction.http://scripts.iucr.org/cgi-bin/paper?S2056989017015523crystal structurebisindoleMRIcontrast agent |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Xin-Hua Lu Hong-Shun Sun Yuan Cai Lu-Lu Chen Yang-Feng Chen |
| spellingShingle |
Xin-Hua Lu Hong-Shun Sun Yuan Cai Lu-Lu Chen Yang-Feng Chen Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) Acta Crystallographica Section E: Crystallographic Communications crystal structure bisindole MRI contrast agent |
| author_facet |
Xin-Hua Lu Hong-Shun Sun Yuan Cai Lu-Lu Chen Yang-Feng Chen |
| author_sort |
Xin-Hua Lu |
| title |
Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) |
| title_short |
Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) |
| title_full |
Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) |
| title_fullStr |
Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) |
| title_full_unstemmed |
Crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1H-indole-2-carboxylate) |
| title_sort |
crystal structure of diethyl 3,3′-[(2-fluorophenyl)methylidene]bis(1h-indole-2-carboxylate) |
| publisher |
International Union of Crystallography |
| series |
Acta Crystallographica Section E: Crystallographic Communications |
| issn |
2056-9890 |
| publishDate |
2017-11-01 |
| description |
In the title compound, C29H25FN2O4, the mean planes of the two indole ring systems (r.m.s. deviations = 0.1392 and 0.0115 Å) are approximately perpendicular to one another, subtending a dihedral angle of 86.0 (5)°; the benzene ring is twisted with respect to the mean planes of the two indole ring systems by 83.3 (2) and 88.1 (4)°, respectively. In the crystal, pairs of N—H...O hydrogen bonds link the molecules into centrosymmetric dimers, which are further linked by N—H...O hydrogen bonds into supramolecular chains propagating along the [101] direction. |
| topic |
crystal structure bisindole MRI contrast agent |
| url |
http://scripts.iucr.org/cgi-bin/paper?S2056989017015523 |
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