Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel

Heavy cold rolling is generally required for efficient grain size refinement in the martensitic reversion process, which is, however, not desirable in practical processing. In the present work, the influence of cold rolling reductions of 32%, 45% and 63% on the microstructure evolution and mechanica...

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Main Authors: Antti Järvenpää, Matias Jaskari, Leo Pentti Karjalainen
Format: Article
Language:English
Published: MDPI AG 2018-02-01
Series:Metals
Subjects:
Online Access:http://www.mdpi.com/2075-4701/8/2/109
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spelling doaj-62b500368d1e4216919a580e28c6acd52020-11-25T01:22:38ZengMDPI AGMetals2075-47012018-02-018210910.3390/met8020109met8020109Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN SteelAntti Järvenpää0Matias Jaskari1Leo Pentti Karjalainen2Kerttu Saalasti Institute, Future Manufacturing Technology Group, University of Oulu, Pajatie 5, FI-85500 Nivala, FinlandKerttu Saalasti Institute, Future Manufacturing Technology Group, University of Oulu, Pajatie 5, FI-85500 Nivala, FinlandCentre for Advanced Steels Research, University of Oulu, P.O. Box 4200, FI-90014 Oulu, FinlandHeavy cold rolling is generally required for efficient grain size refinement in the martensitic reversion process, which is, however, not desirable in practical processing. In the present work, the influence of cold rolling reductions of 32%, 45% and 63% on the microstructure evolution and mechanical properties of a metastable austenitic AISI 301LN type steel were investigated in detail adopting scanning electron microscopy with the electron backscatter diffraction method and mechanical testing. A completely austenitic microstructure and a partially reversed counterpart were created. It was found that the fraction of grains with a size of 3 µm or larger, called medium-sized grains, increased with decreasing the prior cold rolling reduction. These grains are formed mainly from the shear-reversed austenite, transformed from slightly-deformed martensite, by gradual evolution of subgrains to grains. However, in spite of significant amounts of medium-sized grains, the tensile properties after the 32% or 45% cold rolling reductions were practically equal to those after the 63% reduction. The austenite stability against the formation of deformation-induced martensite in subsequent straining was reduced by lowering the cold rolling reduction, due to the larger grain size of medium-sized grains and the shift of their orientation towards {211} <uvw>.http://www.mdpi.com/2075-4701/8/2/109austenitic stainless steelcold rolling reductionreversion treatmentgrain sizetensile propertiesaustenite stability
collection DOAJ
language English
format Article
sources DOAJ
author Antti Järvenpää
Matias Jaskari
Leo Pentti Karjalainen
spellingShingle Antti Järvenpää
Matias Jaskari
Leo Pentti Karjalainen
Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
Metals
austenitic stainless steel
cold rolling reduction
reversion treatment
grain size
tensile properties
austenite stability
author_facet Antti Järvenpää
Matias Jaskari
Leo Pentti Karjalainen
author_sort Antti Järvenpää
title Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
title_short Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
title_full Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
title_fullStr Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
title_full_unstemmed Reversed Microstructures and Tensile Properties after Various Cold Rolling Reductions in AISI 301LN Steel
title_sort reversed microstructures and tensile properties after various cold rolling reductions in aisi 301ln steel
publisher MDPI AG
series Metals
issn 2075-4701
publishDate 2018-02-01
description Heavy cold rolling is generally required for efficient grain size refinement in the martensitic reversion process, which is, however, not desirable in practical processing. In the present work, the influence of cold rolling reductions of 32%, 45% and 63% on the microstructure evolution and mechanical properties of a metastable austenitic AISI 301LN type steel were investigated in detail adopting scanning electron microscopy with the electron backscatter diffraction method and mechanical testing. A completely austenitic microstructure and a partially reversed counterpart were created. It was found that the fraction of grains with a size of 3 µm or larger, called medium-sized grains, increased with decreasing the prior cold rolling reduction. These grains are formed mainly from the shear-reversed austenite, transformed from slightly-deformed martensite, by gradual evolution of subgrains to grains. However, in spite of significant amounts of medium-sized grains, the tensile properties after the 32% or 45% cold rolling reductions were practically equal to those after the 63% reduction. The austenite stability against the formation of deformation-induced martensite in subsequent straining was reduced by lowering the cold rolling reduction, due to the larger grain size of medium-sized grains and the shift of their orientation towards {211} <uvw>.
topic austenitic stainless steel
cold rolling reduction
reversion treatment
grain size
tensile properties
austenite stability
url http://www.mdpi.com/2075-4701/8/2/109
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