5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate

5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate

The asymmetric unit of the title compound, C12H10N4O2S4·2C2H6OS, contains one half of the p-xylene molecule and one dimethyl sulfoxide molecule. The p-xylene molecule is located about a crystallographic inversion centre. In the molecule, the thiadiazole and benzene rings are almost perp...

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Main Authors: Siyoung Jang, Sung Kwon Kang, Nam Sook Cho
Format: Article
Language:English
Published: International Union of Crystallography 2012-03-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812006289
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spelling doaj-62a207dc62104a3bbcc1ac143b3770862020-11-25T02:01:06ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-03-01683o781o78110.1107/S16005368120062895,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvateSiyoung JangSung Kwon KangNam Sook ChoThe asymmetric unit of the title compound, C12H10N4O2S4·2C2H6OS, contains one half of the p-xylene molecule and one dimethyl sulfoxide molecule. The p-xylene molecule is located about a crystallographic inversion centre. In the molecule, the thiadiazole and benzene rings are almost perpendicular to one another, with a dihedral angle of 88.95 (6)°. In the crystal, an N—H...O hydrogen bond is observed between the two components. The dimethyl sulfoxide molecule is disordered over two orientations with an occupancy ratio of 0.879 (1):0.121 (1).http://scripts.iucr.org/cgi-bin/paper?S1600536812006289
collection DOAJ
language English
format Article
sources DOAJ
author Siyoung Jang
Sung Kwon Kang
Nam Sook Cho
spellingShingle Siyoung Jang
Sung Kwon Kang
Nam Sook Cho
5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
Acta Crystallographica Section E
author_facet Siyoung Jang
Sung Kwon Kang
Nam Sook Cho
author_sort Siyoung Jang
title 5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
title_short 5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
title_full 5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
title_fullStr 5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
title_full_unstemmed 5,5′-[1,4-Phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3H)-one] dimethyl sulfoxide disolvate
title_sort 5,5′-[1,4-phenylenebis(methylenesulfanediyl)]bis[1,3,4-thiadiazol-2(3h)-one] dimethyl sulfoxide disolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-03-01
description The asymmetric unit of the title compound, C12H10N4O2S4·2C2H6OS, contains one half of the p-xylene molecule and one dimethyl sulfoxide molecule. The p-xylene molecule is located about a crystallographic inversion centre. In the molecule, the thiadiazole and benzene rings are almost perpendicular to one another, with a dihedral angle of 88.95 (6)°. In the crystal, an N—H...O hydrogen bond is observed between the two components. The dimethyl sulfoxide molecule is disordered over two orientations with an occupancy ratio of 0.879 (1):0.121 (1).
url http://scripts.iucr.org/cgi-bin/paper?S1600536812006289
work_keys_str_mv AT siyoungjang 55amp824214phenylenebismethylenesulfanediylbis134thiadiazol23honedimethylsulfoxidedisolvate
AT sungkwonkang 55amp824214phenylenebismethylenesulfanediylbis134thiadiazol23honedimethylsulfoxidedisolvate
AT namsookcho 55amp824214phenylenebismethylenesulfanediylbis134thiadiazol23honedimethylsulfoxidedisolvate
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