Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide

Crystal structure of 2-benzoylamino-N′-(4-hydroxybenzylidene)-3-(thiophen-2-yl)prop-2-enohydrazide

In the title compound, C21H17N3O3S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34 (6)°]. In the crystal, a combination of N—H...O and...

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Bibliographic Details
Main Authors: Karanth N. Subbulakshmi, Badiadka Narayana, Hemmige S. Yathirajan, Jerry P. Jasinski, Ravindranath S. Rathore, Christopher Glidewell
Format: Article
Language:English
Published: International Union of Crystallography 2016-08-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
supramolecular structure
molecular conformation
hydrogen bonding
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989016010975
Description
Summary:In the title compound, C21H17N3O3S, the non-H atoms, apart from those in the benzoyl group, are almost coplanar (r.m.s. deviation = 0.049 Å) and the benzoyl group is almost orthogonal to the plane of the rest of the molecule [dihedral angle = 80.34 (6)°]. In the crystal, a combination of N—H...O and asymmetric bifurcated O—H...(N,O) hydrogen bonds link the molecules into a three-dimensional network. Weak C—H...O interactions are also observed.
ISSN:2056-9890

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