The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film

Bacterial cellulose (BC) is a natural polymer which have superior properties, like high porosity, high purity, and high permeability. The study objective is to determine the influence of chemical pretreatment on tensile strength and the porosity of BC. The method was to make BC films from pineapple...

Full description

Bibliographic Details
Main Authors: Tito Arif Sutrisno, Heru Suryanto, Retno Wulandari, M. Muhajir, S.M.Shahrul N.S. Zahari
Format: Article
Language:English
Published: Universitas Negeri Malang 2019-08-01
Series:Journal of Mechanical Engineering Science and Technology
Online Access:http://journal2.um.ac.id/index.php/jmest/article/view/7597
id doaj-601e32629d484e6f92b49ffa2bcb986d
record_format Article
spelling doaj-601e32629d484e6f92b49ffa2bcb986d2020-11-25T02:58:47ZengUniversitas Negeri MalangJournal of Mechanical Engineering Science and Technology2580-08172580-24022019-08-013181710.17977/um016v3i12019p0083858The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial FilmTito Arif Sutrisno0Heru Suryanto1Retno Wulandari2M. Muhajir3S.M.Shahrul N.S. Zahari4Master Student of Mechanical Engineering Program, Graduate School, Universitas Negeri MalangMechanical Engineering Department, Engineering Faculty, Universitas Negeri Malang, Jl. Semarang 5, MalangMechanical Engineering Department, Engineering Faculty, Universitas Negeri Malang, Jl. Semarang 5, MalangMaster Student of Mechanical Engineering Program, Graduate School, Universitas Negeri MalangIndustrial Chemical Technology Program, Faculty of Science and Technology, Universiti Sains Islam Malaysia, Bandar Baru Nilai 71800, Negeri Sembilan, MalaysiaBacterial cellulose (BC) is a natural polymer which have superior properties, like high porosity, high purity, and high permeability. The study objective is to determine the influence of chemical pretreatment on tensile strength and the porosity of BC. The method was to make BC films from pineapple peel extract through fermentation process for 14 days. The pretreatment was conducted by immersion of BC in BmimCl, H2O2, and NaOH solution with a concentration of 2.5%; 5%; and 7.5 %, heated at 80 °C then dried in the oven, and the samples were then tested by a tensile test using ASTM-D636-V standard, morphology analysis using Scanning Electron Microscope, and porosity analysis. The results indicate that the tensile strength of control sample was 123 MPa, whereas after chemical pretreatment, the tensile strength was decreased with the greater reduction occurred using NaOH pretreatment compared than the other solutions that having a lower tensile strength of 8.54 MPa at 7.5 % of NaOH. The results of porosity show that the value increased after being treated chemically. The BC film porosity was 87.13% after  NaOH treatment of 7.5% while BC film untreated had porosity of 19.15%. This phenomenon was occurred due to the increasing pore, so the absorption of water increased.http://journal2.um.ac.id/index.php/jmest/article/view/7597
collection DOAJ
language English
format Article
sources DOAJ
author Tito Arif Sutrisno
Heru Suryanto
Retno Wulandari
M. Muhajir
S.M.Shahrul N.S. Zahari
spellingShingle Tito Arif Sutrisno
Heru Suryanto
Retno Wulandari
M. Muhajir
S.M.Shahrul N.S. Zahari
The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
Journal of Mechanical Engineering Science and Technology
author_facet Tito Arif Sutrisno
Heru Suryanto
Retno Wulandari
M. Muhajir
S.M.Shahrul N.S. Zahari
author_sort Tito Arif Sutrisno
title The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
title_short The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
title_full The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
title_fullStr The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
title_full_unstemmed The Effect of Chemical Pretreatment Process on Mechanical Properties and Porosity of Cellulose Bacterial Film
title_sort effect of chemical pretreatment process on mechanical properties and porosity of cellulose bacterial film
publisher Universitas Negeri Malang
series Journal of Mechanical Engineering Science and Technology
issn 2580-0817
2580-2402
publishDate 2019-08-01
description Bacterial cellulose (BC) is a natural polymer which have superior properties, like high porosity, high purity, and high permeability. The study objective is to determine the influence of chemical pretreatment on tensile strength and the porosity of BC. The method was to make BC films from pineapple peel extract through fermentation process for 14 days. The pretreatment was conducted by immersion of BC in BmimCl, H2O2, and NaOH solution with a concentration of 2.5%; 5%; and 7.5 %, heated at 80 °C then dried in the oven, and the samples were then tested by a tensile test using ASTM-D636-V standard, morphology analysis using Scanning Electron Microscope, and porosity analysis. The results indicate that the tensile strength of control sample was 123 MPa, whereas after chemical pretreatment, the tensile strength was decreased with the greater reduction occurred using NaOH pretreatment compared than the other solutions that having a lower tensile strength of 8.54 MPa at 7.5 % of NaOH. The results of porosity show that the value increased after being treated chemically. The BC film porosity was 87.13% after  NaOH treatment of 7.5% while BC film untreated had porosity of 19.15%. This phenomenon was occurred due to the increasing pore, so the absorption of water increased.
url http://journal2.um.ac.id/index.php/jmest/article/view/7597
work_keys_str_mv AT titoarifsutrisno theeffectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT herusuryanto theeffectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT retnowulandari theeffectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT mmuhajir theeffectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT smshahrulnszahari theeffectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT titoarifsutrisno effectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT herusuryanto effectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT retnowulandari effectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT mmuhajir effectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
AT smshahrulnszahari effectofchemicalpretreatmentprocessonmechanicalpropertiesandporosityofcellulosebacterialfilm
_version_ 1724705079326408704