Calcination does not remove all carbon from colloidal nanocrystal assemblies

Synthesis of all-inorganic nanomaterials often relies on organic templates, which are assumed to then be fully removed by calcination. Here, the authors use elastic backscattering spectroscopy to challenge this assumption, finding that calcination leaves behind considerable carbon content that can s...

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Main Authors: Pratyasha Mohapatra, Santosh Shaw, Deyny Mendivelso-Perez, Jonathan M. Bobbitt, Tiago F. Silva, Fabian Naab, Bin Yuan, Xinchun Tian, Emily A. Smith, Ludovico Cademartiri
Format: Article
Language:English
Published: Nature Publishing Group 2017-12-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-017-02267-9
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spelling doaj-5da371945b3840feb5e3b71ee84b8c6b2021-05-11T07:19:13ZengNature Publishing GroupNature Communications2041-17232017-12-01811710.1038/s41467-017-02267-9Calcination does not remove all carbon from colloidal nanocrystal assembliesPratyasha Mohapatra0Santosh Shaw1Deyny Mendivelso-Perez2Jonathan M. Bobbitt3Tiago F. Silva4Fabian Naab5Bin Yuan6Xinchun Tian7Emily A. Smith8Ludovico Cademartiri9Department of Materials Science & Engineering, Iowa State University of Science and TechnologyDepartment of Materials Science & Engineering, Iowa State University of Science and TechnologyDepartment of Chemistry, Iowa State University of Science and TechnologyDepartment of Chemistry, Iowa State University of Science and TechnologyInstituto de Física da Universidade de São PauloMichigan Ion Beam Laboratory, University of MichiganDepartment of Chemical & Biological Engineering, Iowa State University of Science and TechnologyDepartment of Materials Science & Engineering, Iowa State University of Science and TechnologyDepartment of Chemistry, Iowa State University of Science and TechnologyDepartment of Materials Science & Engineering, Iowa State University of Science and TechnologySynthesis of all-inorganic nanomaterials often relies on organic templates, which are assumed to then be fully removed by calcination. Here, the authors use elastic backscattering spectroscopy to challenge this assumption, finding that calcination leaves behind considerable carbon content that can severely affect material function.https://doi.org/10.1038/s41467-017-02267-9
collection DOAJ
language English
format Article
sources DOAJ
author Pratyasha Mohapatra
Santosh Shaw
Deyny Mendivelso-Perez
Jonathan M. Bobbitt
Tiago F. Silva
Fabian Naab
Bin Yuan
Xinchun Tian
Emily A. Smith
Ludovico Cademartiri
spellingShingle Pratyasha Mohapatra
Santosh Shaw
Deyny Mendivelso-Perez
Jonathan M. Bobbitt
Tiago F. Silva
Fabian Naab
Bin Yuan
Xinchun Tian
Emily A. Smith
Ludovico Cademartiri
Calcination does not remove all carbon from colloidal nanocrystal assemblies
Nature Communications
author_facet Pratyasha Mohapatra
Santosh Shaw
Deyny Mendivelso-Perez
Jonathan M. Bobbitt
Tiago F. Silva
Fabian Naab
Bin Yuan
Xinchun Tian
Emily A. Smith
Ludovico Cademartiri
author_sort Pratyasha Mohapatra
title Calcination does not remove all carbon from colloidal nanocrystal assemblies
title_short Calcination does not remove all carbon from colloidal nanocrystal assemblies
title_full Calcination does not remove all carbon from colloidal nanocrystal assemblies
title_fullStr Calcination does not remove all carbon from colloidal nanocrystal assemblies
title_full_unstemmed Calcination does not remove all carbon from colloidal nanocrystal assemblies
title_sort calcination does not remove all carbon from colloidal nanocrystal assemblies
publisher Nature Publishing Group
series Nature Communications
issn 2041-1723
publishDate 2017-12-01
description Synthesis of all-inorganic nanomaterials often relies on organic templates, which are assumed to then be fully removed by calcination. Here, the authors use elastic backscattering spectroscopy to challenge this assumption, finding that calcination leaves behind considerable carbon content that can severely affect material function.
url https://doi.org/10.1038/s41467-017-02267-9
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