Crystal structure of (2-(chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylato–κ2O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N′′,N′′′)nickel(II) perchlorate monohydrate, Ni(C16H36N4)(C12H12O4Cl)ClO4⋅H2O

Crystal structure of (2-(chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylato–κ2O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N′′,N′′′)nickel(II) perchlorate monohydrate, Ni(C16H36N4)(C12H12O4Cl)ClO4⋅H2O

C28H50Cl2N4NiO9, monoclinic, P21/n, a = 10.333(4) Å, b = 26.305(9) Å, c = 12.640(5) Å, β = 102.421(4)°, V = 3355(2) Å3, Z = 4, Rgt(F) = 0.0391, wRref(F2) = 0.1090, T = 296(2) K.

Bibliographic Details
Main Authors: Ou Guang-Chuan, Jia Guo-Kai, Zeng Fei, Tan Ying-zhi, Wang Qiong
Format: Article
Language:English
Published: De Gruyter 2018-05-01
Series:Zeitschrift für Kristallographie - New Crystal Structures
Subjects:
1569958
Online Access:https://doi.org/10.1515/ncrs-2017-0253

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