The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
This work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel pow...
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Series: | Journal of Nanomaterials |
Online Access: | http://dx.doi.org/10.1155/2015/418024 |
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doaj-575ffb6100a842b9bf33ffe04ab4f8b32020-11-24T22:58:13ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292015-01-01201510.1155/2015/418024418024The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel MethodM. Prześniak-Welenc0M. Łapiński1T. Lewandowski2B. Kościelska3L. Wicikowski4W. Sadowski5Faculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandThis work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel powders were annealed at various temperatures ranging from 100°C to 600°C. The structure of the samples was characterized by X-ray diffraction method (XRD), scanning electron microscope (SEM), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and mass spectroscopy (MS). The rod-like structure of V2O5 was obtained at 600°C on both quartz glass and silicon substrates and also from the bulk xerogel. The growth process and the effect of annealing treatment on the nanostructure are briefly discussed.http://dx.doi.org/10.1155/2015/418024 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
M. Prześniak-Welenc M. Łapiński T. Lewandowski B. Kościelska L. Wicikowski W. Sadowski |
spellingShingle |
M. Prześniak-Welenc M. Łapiński T. Lewandowski B. Kościelska L. Wicikowski W. Sadowski The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method Journal of Nanomaterials |
author_facet |
M. Prześniak-Welenc M. Łapiński T. Lewandowski B. Kościelska L. Wicikowski W. Sadowski |
author_sort |
M. Prześniak-Welenc |
title |
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method |
title_short |
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method |
title_full |
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method |
title_fullStr |
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method |
title_full_unstemmed |
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method |
title_sort |
influence of thermal conditions on v2o5 nanostructures prepared by sol-gel method |
publisher |
Hindawi Limited |
series |
Journal of Nanomaterials |
issn |
1687-4110 1687-4129 |
publishDate |
2015-01-01 |
description |
This work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel powders were annealed at various temperatures ranging from 100°C to 600°C. The structure of the samples was characterized by X-ray diffraction method (XRD), scanning electron microscope (SEM), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and mass spectroscopy (MS). The rod-like structure of V2O5 was obtained at 600°C on both quartz glass and silicon substrates and also from the bulk xerogel. The growth process and the effect of annealing treatment on the nanostructure are briefly discussed. |
url |
http://dx.doi.org/10.1155/2015/418024 |
work_keys_str_mv |
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