The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method

This work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel pow...

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Main Authors: M. Prześniak-Welenc, M. Łapiński, T. Lewandowski, B. Kościelska, L. Wicikowski, W. Sadowski
Format: Article
Language:English
Published: Hindawi Limited 2015-01-01
Series:Journal of Nanomaterials
Online Access:http://dx.doi.org/10.1155/2015/418024
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spelling doaj-575ffb6100a842b9bf33ffe04ab4f8b32020-11-24T22:58:13ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292015-01-01201510.1155/2015/418024418024The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel MethodM. Prześniak-Welenc0M. Łapiński1T. Lewandowski2B. Kościelska3L. Wicikowski4W. Sadowski5Faculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandFaculty of Applied Physics and Mathematics, Gdańsk University of Technology, Narutowicza 11/12, 80-233 Gdańsk, PolandThis work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel powders were annealed at various temperatures ranging from 100°C to 600°C. The structure of the samples was characterized by X-ray diffraction method (XRD), scanning electron microscope (SEM), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and mass spectroscopy (MS). The rod-like structure of V2O5 was obtained at 600°C on both quartz glass and silicon substrates and also from the bulk xerogel. The growth process and the effect of annealing treatment on the nanostructure are briefly discussed.http://dx.doi.org/10.1155/2015/418024
collection DOAJ
language English
format Article
sources DOAJ
author M. Prześniak-Welenc
M. Łapiński
T. Lewandowski
B. Kościelska
L. Wicikowski
W. Sadowski
spellingShingle M. Prześniak-Welenc
M. Łapiński
T. Lewandowski
B. Kościelska
L. Wicikowski
W. Sadowski
The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
Journal of Nanomaterials
author_facet M. Prześniak-Welenc
M. Łapiński
T. Lewandowski
B. Kościelska
L. Wicikowski
W. Sadowski
author_sort M. Prześniak-Welenc
title The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
title_short The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
title_full The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
title_fullStr The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
title_full_unstemmed The Influence of Thermal Conditions on V2O5 Nanostructures Prepared by Sol-Gel Method
title_sort influence of thermal conditions on v2o5 nanostructures prepared by sol-gel method
publisher Hindawi Limited
series Journal of Nanomaterials
issn 1687-4110
1687-4129
publishDate 2015-01-01
description This work presents the result of structure investigations of V2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel powders were annealed at various temperatures ranging from 100°C to 600°C. The structure of the samples was characterized by X-ray diffraction method (XRD), scanning electron microscope (SEM), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and mass spectroscopy (MS). The rod-like structure of V2O5 was obtained at 600°C on both quartz glass and silicon substrates and also from the bulk xerogel. The growth process and the effect of annealing treatment on the nanostructure are briefly discussed.
url http://dx.doi.org/10.1155/2015/418024
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