Methyl 4-methylsulfonyl-2-nitrobenzoate

Methyl 4-methylsulfonyl-2-nitrobenzoate

The title compound, C9H9NO6S, was prepared by the reaction of methanol and thionyl chloride with 4-methylsulfonyl-2-nitrobenzoic acid under mild conditions. The dihedral angle between the nitro group and benzene ring is 21.33 (19)° and that between the carboxylate group an...

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Main Authors: Yan-Jun Hou, Wen-Yi Chu, Jun Sui, Zhi-Zhong Sun
Format: Article
Language:English
Published: International Union of Crystallography 2010-07-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810021914
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spelling doaj-561f7e7c7391435ba4607b9515cd41262020-11-24T22:08:40ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682010-07-01667o1669o166910.1107/S1600536810021914Methyl 4-methylsulfonyl-2-nitrobenzoateYan-Jun HouWen-Yi ChuJun SuiZhi-Zhong SunThe title compound, C9H9NO6S, was prepared by the reaction of methanol and thionyl chloride with 4-methylsulfonyl-2-nitrobenzoic acid under mild conditions. The dihedral angle between the nitro group and benzene ring is 21.33 (19)° and that between the carboxylate group and the benzene ring is 72.09 (17)°. The crystal structure is stabilized by weak intermolecular bifurcated C—H...O interactions occurring in the (100) plane. http://scripts.iucr.org/cgi-bin/paper?S1600536810021914
collection DOAJ
language English
format Article
sources DOAJ
author Yan-Jun Hou
Wen-Yi Chu
Jun Sui
Zhi-Zhong Sun
spellingShingle Yan-Jun Hou
Wen-Yi Chu
Jun Sui
Zhi-Zhong Sun
Methyl 4-methylsulfonyl-2-nitrobenzoate
Acta Crystallographica Section E
author_facet Yan-Jun Hou
Wen-Yi Chu
Jun Sui
Zhi-Zhong Sun
author_sort Yan-Jun Hou
title Methyl 4-methylsulfonyl-2-nitrobenzoate
title_short Methyl 4-methylsulfonyl-2-nitrobenzoate
title_full Methyl 4-methylsulfonyl-2-nitrobenzoate
title_fullStr Methyl 4-methylsulfonyl-2-nitrobenzoate
title_full_unstemmed Methyl 4-methylsulfonyl-2-nitrobenzoate
title_sort methyl 4-methylsulfonyl-2-nitrobenzoate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2010-07-01
description The title compound, C9H9NO6S, was prepared by the reaction of methanol and thionyl chloride with 4-methylsulfonyl-2-nitrobenzoic acid under mild conditions. The dihedral angle between the nitro group and benzene ring is 21.33 (19)° and that between the carboxylate group and the benzene ring is 72.09 (17)°. The crystal structure is stabilized by weak intermolecular bifurcated C—H...O interactions occurring in the (100) plane.
url http://scripts.iucr.org/cgi-bin/paper?S1600536810021914
work_keys_str_mv AT yanjunhou methyl4methylsulfonyl2nitrobenzoate
AT wenyichu methyl4methylsulfonyl2nitrobenzoate
AT junsui methyl4methylsulfonyl2nitrobenzoate
AT zhizhongsun methyl4methylsulfonyl2nitrobenzoate
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