Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements

The preparation, certification, and characterization of two new biological certified reference materials for inorganic trace analysis have been presented. They are based on two different varieties of tobacco leaves, namely, Oriental Basma Tobacco Leaves (INCT-OBTL-5), grown in Greece, and Polish Vir...

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Main Authors: Zbigniew Samczyński, Rajmund S. Dybczyński, Halina Polkowska-Motrenko, Ewelina Chajduk, Marta Pyszynska, Bożena Danko, Elżbieta Czerska, Krzysztof Kulisa, Katarzyna Doner, Paweł Kalbarczyk
Format: Article
Language:English
Published: Hindawi Limited 2012-01-01
Series:The Scientific World Journal
Online Access:http://dx.doi.org/10.1100/2012/216380
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spelling doaj-4c406cda1a2d4bc68e6861d1e2532d762020-11-25T00:46:30ZengHindawi LimitedThe Scientific World Journal1537-744X2012-01-01201210.1100/2012/216380216380Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential ElementsZbigniew Samczyński0Rajmund S. Dybczyński1Halina Polkowska-Motrenko2Ewelina Chajduk3Marta Pyszynska4Bożena Danko5Elżbieta Czerska6Krzysztof Kulisa7Katarzyna Doner8Paweł Kalbarczyk9Laboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandLaboratory of Nuclear Analytical Methods, Institute of Nuclear Chemistry and Technology, Dorodna 16, 03-195 Warsaw, PolandThe preparation, certification, and characterization of two new biological certified reference materials for inorganic trace analysis have been presented. They are based on two different varieties of tobacco leaves, namely, Oriental Basma Tobacco Leaves (INCT-OBTL-5), grown in Greece, and Polish Virginia Tobacco Leaves (INCT-PVTL-6), grown in Poland. Certification of the materials was based on the statistical evaluation of results obtained in a worldwide interlaboratory comparison, in which 87 laboratories from 18 countries participated, providing 2568 laboratory averages on nearly 80 elements. It was possible to establish the certified values of concentration for many elements in the new materials, that is, 37 in INCT-OBTL-5 and 36 in INCT-PVTL-6, including several toxic ones like As, Cd, Hg, Pb, and so forth. The share and the role of instrumental analytical techniques used in the process of certification of the new CRMs are discussed.http://dx.doi.org/10.1100/2012/216380
collection DOAJ
language English
format Article
sources DOAJ
author Zbigniew Samczyński
Rajmund S. Dybczyński
Halina Polkowska-Motrenko
Ewelina Chajduk
Marta Pyszynska
Bożena Danko
Elżbieta Czerska
Krzysztof Kulisa
Katarzyna Doner
Paweł Kalbarczyk
spellingShingle Zbigniew Samczyński
Rajmund S. Dybczyński
Halina Polkowska-Motrenko
Ewelina Chajduk
Marta Pyszynska
Bożena Danko
Elżbieta Czerska
Krzysztof Kulisa
Katarzyna Doner
Paweł Kalbarczyk
Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
The Scientific World Journal
author_facet Zbigniew Samczyński
Rajmund S. Dybczyński
Halina Polkowska-Motrenko
Ewelina Chajduk
Marta Pyszynska
Bożena Danko
Elżbieta Czerska
Krzysztof Kulisa
Katarzyna Doner
Paweł Kalbarczyk
author_sort Zbigniew Samczyński
title Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
title_short Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
title_full Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
title_fullStr Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
title_full_unstemmed Two New Reference Materials Based on Tobacco Leaves: Certification for over a Dozen of Toxic and Essential Elements
title_sort two new reference materials based on tobacco leaves: certification for over a dozen of toxic and essential elements
publisher Hindawi Limited
series The Scientific World Journal
issn 1537-744X
publishDate 2012-01-01
description The preparation, certification, and characterization of two new biological certified reference materials for inorganic trace analysis have been presented. They are based on two different varieties of tobacco leaves, namely, Oriental Basma Tobacco Leaves (INCT-OBTL-5), grown in Greece, and Polish Virginia Tobacco Leaves (INCT-PVTL-6), grown in Poland. Certification of the materials was based on the statistical evaluation of results obtained in a worldwide interlaboratory comparison, in which 87 laboratories from 18 countries participated, providing 2568 laboratory averages on nearly 80 elements. It was possible to establish the certified values of concentration for many elements in the new materials, that is, 37 in INCT-OBTL-5 and 36 in INCT-PVTL-6, including several toxic ones like As, Cd, Hg, Pb, and so forth. The share and the role of instrumental analytical techniques used in the process of certification of the new CRMs are discussed.
url http://dx.doi.org/10.1100/2012/216380
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