(±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate

(±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate

The title compound, C24H14O9·2CH3OH, displays a chair-shaped form. The two dihydroindenone ring systems are located above and below the central fused-ring system, the dihedral angles between the mean planes of dihydroindenone ring systems and the mean plane of central fused-ring system are 67.91 (5)...

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Main Authors: Maayan Gil, Joseph Almog, Faina Dubnikova, Benny Bogoslavski, Shmuel Cohen
Format: Article
Language:English
Published: International Union of Crystallography 2014-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536814006643
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spelling doaj-48609472a7da489fa77d482afe708c352020-11-24T21:47:11ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-05-01705o506o50610.1107/S1600536814006643xu5780(±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvateMaayan Gil0Joseph Almog1Faina Dubnikova2Benny Bogoslavski3Shmuel Cohen4The Institute of Chemistry, The Hebrew University of Jerusalem, Jerusalem 91904, IsraelThe Institute of Chemistry, The Hebrew University of Jerusalem, Jerusalem 91904, IsraelThe Institute of Chemistry, The Hebrew University of Jerusalem, Jerusalem 91904, IsraelThe Institute of Chemistry, The Hebrew University of Jerusalem, Jerusalem 91904, IsraelThe Institute of Chemistry, The Hebrew University of Jerusalem, Jerusalem 91904, IsraelThe title compound, C24H14O9·2CH3OH, displays a chair-shaped form. The two dihydroindenone ring systems are located above and below the central fused-ring system, the dihedral angles between the mean planes of dihydroindenone ring systems and the mean plane of central fused-ring system are 67.91 (5) and 73.52 (4)°, respectively. In the crystal, extensive O—H...O hydrogen bonds, weak C—H...O hydrogen bonds and C—H...π interactions link the molecules into a three-dimensional supramolecular architecture.http://scripts.iucr.org/cgi-bin/paper?S1600536814006643
collection DOAJ
language English
format Article
sources DOAJ
author Maayan Gil
Joseph Almog
Faina Dubnikova
Benny Bogoslavski
Shmuel Cohen
spellingShingle Maayan Gil
Joseph Almog
Faina Dubnikova
Benny Bogoslavski
Shmuel Cohen
(±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
Acta Crystallographica Section E
author_facet Maayan Gil
Joseph Almog
Faina Dubnikova
Benny Bogoslavski
Shmuel Cohen
author_sort Maayan Gil
title (±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
title_short (±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
title_full (±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
title_fullStr (±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
title_full_unstemmed (±)-4,12,15,18,26-Pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
title_sort (±)-4,12,15,18,26-pentahydroxy-13,17-dioxaheptacyclo[14.10.0.03,14.04,12.06,11.018,26.019,24]hexacosa-1,3(14),6(11),7,9,15,19,21,23-nonaene-5,25-dione methanol disolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2014-05-01
description The title compound, C24H14O9·2CH3OH, displays a chair-shaped form. The two dihydroindenone ring systems are located above and below the central fused-ring system, the dihedral angles between the mean planes of dihydroindenone ring systems and the mean plane of central fused-ring system are 67.91 (5) and 73.52 (4)°, respectively. In the crystal, extensive O—H...O hydrogen bonds, weak C—H...O hydrogen bonds and C—H...π interactions link the molecules into a three-dimensional supramolecular architecture.
url http://scripts.iucr.org/cgi-bin/paper?S1600536814006643
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AT josephalmog 412151826pentahydroxy1317dioxaheptacyclo141000314041206110182601924hexacosa13146117915192123nonaene525dionemethanoldisolvate
AT fainadubnikova 412151826pentahydroxy1317dioxaheptacyclo141000314041206110182601924hexacosa13146117915192123nonaene525dionemethanoldisolvate
AT bennybogoslavski 412151826pentahydroxy1317dioxaheptacyclo141000314041206110182601924hexacosa13146117915192123nonaene525dionemethanoldisolvate
AT shmuelcohen 412151826pentahydroxy1317dioxaheptacyclo141000314041206110182601924hexacosa13146117915192123nonaene525dionemethanoldisolvate
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