Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
ZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method,...
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Series: | Journal of Nanomaterials |
Online Access: | http://dx.doi.org/10.1155/2013/903191 |
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doaj-483ad41f36054aadad1a6fe3163014b42020-11-24T22:49:12ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292013-01-01201310.1155/2013/903191903191Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating TechniqueJose Alberto Alvarado0A. Maldonado1H. Juarez2M. Pacio3Centro de Investigaciones y de Estudios Avanzados del Instituto Politecnico Nacional, Programa de Nanociencias y Nanotecnología, Avenida Instituto Politécnico Nacional No. 2508, Col. San Pedro Zacatenco, C.P. 07360, MexicoCentro de Investigaciones y de Estudios Avanzados del Instituto Politecnico Nacional (CINVESTAV-IPN), Seccion de Electronica del Estado Solido, Avenida Instituto Politécnico Nacional No. 2508, Col. San Pedro Zacatenco, C.P. 07360, MexicoCentro de Investigaciones en Dispositivos Semiconductores, Benemérita Universidad Autónoma de Puebla, Ciudad Universitaria Avenida San Claudio y 14 Sur, 72570 Puebla, MexicoCentro de Investigaciones en Dispositivos Semiconductores, Benemérita Universidad Autónoma de Puebla, Ciudad Universitaria Avenida San Claudio y 14 Sur, 72570 Puebla, MexicoZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method, and we do not use any alkanes to remove the byproducts; only a centrifuge to remove those ones was used, thereby the stabilization increases up to 24 days. It is observed from the results that only three times of washing is enough to prevent the rapid aging process. The effect of annealing process on the composition, size, and geometrical shape of ZnO nanoparticles was studied in order to know whether the annealing process affects the crystallization and growth of the nanoparticles. After the synthesis, the colloidal nanoparticles were deposited by spin coating technique showing that the formed nanoparticles have no uniformly deposition pattern. But is possible to deposit those ones in glass substrates. A possible deposition process of the nanoparticles is proposed.http://dx.doi.org/10.1155/2013/903191 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Jose Alberto Alvarado A. Maldonado H. Juarez M. Pacio |
spellingShingle |
Jose Alberto Alvarado A. Maldonado H. Juarez M. Pacio Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique Journal of Nanomaterials |
author_facet |
Jose Alberto Alvarado A. Maldonado H. Juarez M. Pacio |
author_sort |
Jose Alberto Alvarado |
title |
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique |
title_short |
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique |
title_full |
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique |
title_fullStr |
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique |
title_full_unstemmed |
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique |
title_sort |
synthesis of colloidal zno nanoparticles and deposit of thin films by spin coating technique |
publisher |
Hindawi Limited |
series |
Journal of Nanomaterials |
issn |
1687-4110 1687-4129 |
publishDate |
2013-01-01 |
description |
ZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method, and we do not use any alkanes to remove the byproducts; only a centrifuge to remove those ones was used, thereby the stabilization increases up to 24 days. It is observed from the results that only three times of washing is enough to prevent the rapid aging process. The effect of annealing process on the composition, size, and geometrical shape of ZnO nanoparticles was studied in order to know whether the annealing process affects the crystallization and growth of the nanoparticles. After the synthesis, the colloidal nanoparticles were deposited by spin coating technique showing that the formed nanoparticles have no uniformly deposition pattern. But is possible to deposit those ones in glass substrates. A possible deposition process of the nanoparticles is proposed. |
url |
http://dx.doi.org/10.1155/2013/903191 |
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