Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique

ZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method,...

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Main Authors: Jose Alberto Alvarado, A. Maldonado, H. Juarez, M. Pacio
Format: Article
Language:English
Published: Hindawi Limited 2013-01-01
Series:Journal of Nanomaterials
Online Access:http://dx.doi.org/10.1155/2013/903191
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spelling doaj-483ad41f36054aadad1a6fe3163014b42020-11-24T22:49:12ZengHindawi LimitedJournal of Nanomaterials1687-41101687-41292013-01-01201310.1155/2013/903191903191Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating TechniqueJose Alberto Alvarado0A. Maldonado1H. Juarez2M. Pacio3Centro de Investigaciones y de Estudios Avanzados del Instituto Politecnico Nacional, Programa de Nanociencias y Nanotecnología, Avenida Instituto Politécnico Nacional No. 2508, Col. San Pedro Zacatenco, C.P. 07360, MexicoCentro de Investigaciones y de Estudios Avanzados del Instituto Politecnico Nacional (CINVESTAV-IPN), Seccion de Electronica del Estado Solido, Avenida Instituto Politécnico Nacional No. 2508, Col. San Pedro Zacatenco, C.P. 07360, MexicoCentro de Investigaciones en Dispositivos Semiconductores, Benemérita Universidad Autónoma de Puebla, Ciudad Universitaria Avenida San Claudio y 14 Sur, 72570 Puebla, MexicoCentro de Investigaciones en Dispositivos Semiconductores, Benemérita Universidad Autónoma de Puebla, Ciudad Universitaria Avenida San Claudio y 14 Sur, 72570 Puebla, MexicoZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method, and we do not use any alkanes to remove the byproducts; only a centrifuge to remove those ones was used, thereby the stabilization increases up to 24 days. It is observed from the results that only three times of washing is enough to prevent the rapid aging process. The effect of annealing process on the composition, size, and geometrical shape of ZnO nanoparticles was studied in order to know whether the annealing process affects the crystallization and growth of the nanoparticles. After the synthesis, the colloidal nanoparticles were deposited by spin coating technique showing that the formed nanoparticles have no uniformly deposition pattern. But is possible to deposit those ones in glass substrates. A possible deposition process of the nanoparticles is proposed.http://dx.doi.org/10.1155/2013/903191
collection DOAJ
language English
format Article
sources DOAJ
author Jose Alberto Alvarado
A. Maldonado
H. Juarez
M. Pacio
spellingShingle Jose Alberto Alvarado
A. Maldonado
H. Juarez
M. Pacio
Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
Journal of Nanomaterials
author_facet Jose Alberto Alvarado
A. Maldonado
H. Juarez
M. Pacio
author_sort Jose Alberto Alvarado
title Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
title_short Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
title_full Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
title_fullStr Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
title_full_unstemmed Synthesis of Colloidal ZnO Nanoparticles and Deposit of Thin Films by Spin Coating Technique
title_sort synthesis of colloidal zno nanoparticles and deposit of thin films by spin coating technique
publisher Hindawi Limited
series Journal of Nanomaterials
issn 1687-4110
1687-4129
publishDate 2013-01-01
description ZnO colloidal nanoparticles were synthesized, the average size of these nanoparticles is around 25 nm with hexagonal form. It was noted that stabilization depends directly on the purifying process; in this work we do not change the nature of the solution as a difference from Meulekamp's method, and we do not use any alkanes to remove the byproducts; only a centrifuge to remove those ones was used, thereby the stabilization increases up to 24 days. It is observed from the results that only three times of washing is enough to prevent the rapid aging process. The effect of annealing process on the composition, size, and geometrical shape of ZnO nanoparticles was studied in order to know whether the annealing process affects the crystallization and growth of the nanoparticles. After the synthesis, the colloidal nanoparticles were deposited by spin coating technique showing that the formed nanoparticles have no uniformly deposition pattern. But is possible to deposit those ones in glass substrates. A possible deposition process of the nanoparticles is proposed.
url http://dx.doi.org/10.1155/2013/903191
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